Synthesis and Characterization of Single Crystal of bis-(L-Histidinato)nickel(II) Monohydrate

被引：2

作者：

Hashemian, Saeedeh ^{[1
]}

机构：

[1] Islamic Azad Univ, Yazd Branch, Dept Chem, Yazd, Iran

来源：

ASIAN JOURNAL OF CHEMISTRY | 2013年 / 25卷 / 05期

关键词：

Synthesis; Characterization; Single crystal; Bis-(L-histidinato)nickel(II) monohydrate; COMPLEXES;

D O I：

10.14233/ajchem.2013.13409A

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The complex bis-(L-histidinato)nickel(II) monohydrate has been synthesized and structurally characterized by single-crystal X-ray diffraction. This complex was solved in the monoclinic system, space group C2, with the following unit-cell parameters: a = 29.313(6) angstrom, b = 8.227 (2)angstrom, c = 6.264(1) angstrom, alpha = 90 degrees, beta = 90.189(5)degrees, gamma = 90 degrees, Z = 4, V = 1510.5(5)degrees A(3). The final R value was R1 = 0.0301 for 7558 measured reflections.

引用

页码：2925 / 2926

页数：2

共 4 条

[1] Ni(II) complexes of dipeptides: a thermodynamic and spectroscopic study
Conato, C
Ferrari, S
Kozlowski, H
Pulidori, F
Remelli, M
[J]. POLYHEDRON, 2001, 20 (7-8) : 615 - 621
[2] Formation equilibria of nickel complexes with glycyl-histidyl-lysine and two synthetic analogues
Conato, C
Kozlowski, H
Swiatek-Kozlowska, J
Mlynarz, P
Remelli, M
Silvestri, S
[J]. JOURNAL OF INORGANIC BIOCHEMISTRY, 2004, 98 (01) : 153 - 160
[3] Laura E., 2006, J INORG BIOCHEM, V192, P100
[4] Sheldrick G., 1998, SHELXL 97 PROGRAMS C

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