Crystal structure of bis(tetrabutylammonium) bis(1,2,3-trioxocyclopent-4-ene-4,5-dithiolato-S,S′)mercury(II) - water (1:0.28), [N(C4H9)4]2[Hg(C5O3S2)2] • 0.28H2O

被引：0

作者：

Zhang, Xi-Man ^{[1
]}

Li, Ping ^{[1
]}

Wang, Hai ^{[1
]}

Chen, Hong-Yu ^{[1
]}

机构：

[1] Taishan Med Univ, Sch Chem & Chem Engn, Tai An 271016, Shandong, Peoples R China

来源：

ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2012年 / 227卷 / 02期

关键词：

DITHIOCROCONATE; SALTS;

D O I：

10.1524/ncrs.2012.0104

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

C42H72.56HgN2O6.28S4, triclinic, P (1) over bar (no. 2), a = 9.787(5) angstrom, b = 14.999(5) angstrom, c = 17.342(5) angstrom, alpha = 74.973(5)degrees, beta = 87.124(5)degrees, gamma = 87.609(5)degrees, V = 2454.5 angstrom(3), Z = 2, R-gt(F) = 0.036, wR(ref)(F-2) = 0.073, T = 293 K.

引用

页码：230 / 232

页数：3

共 9 条

[1] SIR97:: a new tool for crystal structure determination and refinement
Altomare, A
Burla, MC
Camalli, M
Cascarano, GL
Giacovazzo, C
Guagliardi, A
Moliterni, AGG
Polidori, G
Spagna, R
[J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1999, 32 : 115 - 119
[2] Bis(tetrabutylammonium) bis(3,4,5-trioxocyclopent-1-ene-1,2-dithiolato-κ2S,S′)cadmate(II) 0.25-hydrate
Chen, Hong-Yu
Xia, Guang-Ming
Zhang, Zhen-Wei
Li, Ping
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : M12 - U278
[3] Synthesis, crystal structure and properties of the semiconducting salts (TTF)2[Ni(dtcr)2] and (ET)2[Ni(dtcr)2] based on [Ni(dtcr)2] dianions (dtcr = dithiocroconate)
Deplano, P
Faulmann, C
Mercuri, ML
Pilia, L
Salidu, M
Serpe, A
[J]. DALTON TRANSACTIONS, 2006, (20) : 2456 - 2462
[4] Deplano P, 2005, EUR J INORG CHEM, P1829
[5] Farrugia L. J., 1999, Journal of Applied Crystallography, V32, P837, DOI [DOI 10.1107/S0021889812029111, 10.1107/S0021889899006020, DOI 10.1107/S0021889899006020]
[6] Gunther S., 1992, CHEM REV, V92, P1227
[7] Synthesis and characterization of metal tris-dithiocroconate complexes and dicyanomethylene-substituted analogues. Crystal and molecular structure of [Ph(4)P](3)[Co(dtcroc)(3)]center dot 0.6acetone
Heuer, WB
Pearson, WH
[J]. POLYHEDRON, 1996, 15 (13) : 2199 - 2210
[8] Raymond F. X. W., 1976, PHOSPHORUS SULFUR, V2, P141
[9] A short history of SHELX
Sheldrick, George M.
[J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122

← 1 →