KOTOBUKI-1 apparatus for cryogenic coherent X-ray diffraction imaging

被引：29

作者：

Nakasako, Masayoshi ^{[1
,2
]}

Takayama, Yuki ^{[1
,2
]}

Oroguchi, Tomotaka ^{[1
,2
]}

Sekiguchi, Yuki ^{[1
,2
]}

Kobayashi, Amane ^{[1
,2
]}

Shirahama, Keiya ^{[1
]}

Yamamoto, Masaki ^{[2
]}

Hikima, Takaaki ^{[2
]}

Yonekura, Koji ^{[2
]}

Maki-Yonekura, Saori ^{[2
]}

Kohmura, Yoshiki ^{[2
]}

Inubushi, Yuichi ^{[2
]}

Takahashi, Yukio ^{[2
,3
]}

Suzuki, Akihiro ^{[2
,3
]}

Matsunaga, Sachihiro ^{[4
]}

Inui, Yayoi ^{[4
]}

Tono, Kensuke ^{[5
]}

Kameshima, Takashi ^{[5
]}

Joti, Yasumasa ^{[5
]}

Hoshi, Takahiko ^{[6
]}

机构：

[1] Keio Univ, Fac Sci & Technol, Dept Phys, Kohoku Ku, Yokohama, Kanagawa 2238522, Japan

[2] RIKEN SPring 8 Ctr, Sayo, Hyogo 6795148, Japan

[3] Osaka Univ, Grad Sch Engn, Dept Precis Sci & Technol, Suita, Osaka 5650871, Japan

[4] Tokyo Univ Sci, Fac Sci & Technol, Dept Appl Biol Sci, Noda, Chiba 2788510, Japan

[5] Japan Synchrotron Radiat Res Inst, Sayo, Hyogo 6795198, Japan

[6] Kohzu Precis Co Ltd, Aso Ku, Kawasaki, Kanagawa 2158521, Japan

来源：

REVIEW OF SCIENTIFIC INSTRUMENTS | 2013年 / 84卷 / 09期

关键词：

FREE-ELECTRON LASER; RADIATION-DAMAGE; PHASE RETRIEVAL; PROTEIN CRYSTALS; MICROSCOPY; CRYSTALLOGRAPHY; SPECIMENS; RESOLUTION; CHLOROPLAST; DIVISION;

D O I：

10.1063/1.4822123

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

We have developed an experimental apparatus named KOTOBUKI-1 for use in coherent X-ray diffraction imaging experiments of frozen-hydrated non-crystalline particles at cryogenic temperature. For cryogenic specimen stage with small positional fluctuation for a long exposure time of more than several minutes, we here use a cryogenic pot cooled by the evaporation cooling effect for liquid nitrogen. In addition, a loading device is developed to bring specimens stored in liquid nitrogen to the specimen stage in vacuum. The apparatus allows diffraction data collection for frozen-hydrated specimens at 66 K with a positional fluctuation of less than 0.4 mu m and provides an experimental environment to easily exchange specimens from liquid nitrogen storage to the specimen stage. The apparatus was developed and utilized in diffraction data collection of non-crystalline particles with dimensions of mu m from material and biological sciences, such as metal colloid particles and chloroplast, at BL29XU of SPring-8. Recently, it has been applied for single-shot diffraction data collection of non-crystalline particles with dimensions of sub-mu m using X-ray free electron laser at BL3 of SACLA. (C) 2013 AIP Publishing LLC.

引用

页数：11

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