A simple and efficient synthesis of 3,4-dihydropyrimidin-2-(1H)-ones via Biginelli reaction catalyzed by nanomagnetic-supported sulfonic acid

被引：98
作者：
Kolvari, Eskandar [1 ]
Koukabi, Nadiya [1 ]
Armandpour, Ozra [1 ]
机构：
[1] Semnan Univ, Dept Chem, Semnan 3535119111, Iran
来源：
TETRAHEDRON | 2014年 / 70卷 / 06期
关键词：
Nanomagnetic catalyst; Heterogeneous catalyst; Solvent-free route; Microwave irradiation; ONE-POT SYNTHESIS; REUSABLE CATALYST; IONIC LIQUID; DIHYDROPYRIMIDINONES; PROTOCOL; THIONES;
D O I：
10.1016/j.tet.2013.10.085
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Nanomagnetic-supported sulfonic acid is found to be a new, powerful, and reusable heterogeneous catalyst for the rapid synthesis of 3,4-dihydropyrimidin-2-(1H)-ones under conventional heating and microwave irradiation. This is the first example of combination of magnetic iron nanoparticles and microwave technique for the multicomponent reaction. The optical behaviors of the 3,4-dihydropyrimidin-2-(1H)-ones have been investigated by UV-vis spectroscopy. (C) 2013 Elsevier Ltd. All rights reserved.
引用
收藏
页码：1383 / 1386
页数：4
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