High yield synthesis of 5,5′-dimethyl-2,2′-bipyridine and 5,5"-dimethyl-2,2′:6′,2"-terpyridine and some bisfunctionalization reactions using N-bromosuccinimide

被引：0
|
作者：
Schubert, US [1 ]
Eschbaumer, C [1 ]
Hochwimmer, G [1 ]
机构：
[1] Tech Univ Munich, Lehrstuhl Makromol Stoffe, D-85747 Garching, Germany
来源：
SYNTHESIS-STUTTGART | 1999年 / 05期
关键词：
2,2 '-bipyridines; 2,2 ': 6 ',2 ''-terpyridines; Stille coupling; organotin intermediates; radical bromination;
D O I：
暂无
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
5,5'-Dimethyl-2,2'-bipyridine and 5,5 "-dimethyl-2,2':6',2 "-terpyridine were synthesized in multigram quantities in high yields utilizing organotin intermediates and Stille coupling procedures. The obtained ligands were dibrominated using N-bromosuccinimide.
引用
收藏
页码：779 / 782
页数：4
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