N,N-Bis(quinolin-8-yl)-2,2′-[(1,3,4-thiadiazole-2,5-diyl)bis(sulfanediyl)]diacetamide monohydrate

被引:1
作者
Li, Xiao-Feng [2 ]
An, Yan [2 ]
Huang, Qing-Hua [1 ]
Wen, Yong-Hong [1 ]
机构
[1] Qingdao Univ Sci & Technol, Coll Chem & Mol Engn, Qingdao 266042, Peoples R China
[2] Shanghai Maritime Univ, Inst Marine Mat Sci & Engn, Shanghai 201305, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词
data-to-parameter ratio = 13.6; mean σ(C-C) = 0.003 Å; R factor = 0.044; single-crystal X-ray study; T = 293 K; wR factor = 0.109;
D O I
10.1107/S1600536811047222
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C24H18N6O2S3 center dot H2O, the thiadiazole ring makes dihedral angles of 78.00 (13) and 77.27 (13)degrees with the quinoline ring systems. In the crystal, molecules are linked into a two-dimensional network by O-H center dot center dot center dot O and C-H center dot center dot center dot O hydrogen bonds.
引用
收藏
页码:O3291 / U510
页数:12
相关论文
共 7 条
[1]  
Bruker, 2001, APEX2 SAINT
[2]  
Gurn N, 2001, J SCI IND RES INDIA, V60, P601
[3]  
Sheldrick G.M., 1996, SADABS
[4]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[5]   Carbonic anhydrase inhibitors: Inhibition of the tumor-associated isozyme IX with aromatic and heterocyclic sulfonamides [J].
Vullo, D ;
Franchi, M ;
Gallori, E ;
Pastorek, J ;
Scozzafava, A ;
Pastorekova, S ;
Supuran, CT .
BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2003, 13 (06) :1005-1009
[6]   N,N′-Diphenyl-2,2′-(1,3,4-thiadiazolyl-2,5-dithio)-diacetamide [J].
Wen, YH ;
Zhang, SS ;
Yu, BH ;
Li, XM ;
Liu, Q .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 :O347-O348
[7]  
Zhang SS, 2005, INDIAN J HETEROCY CH, V15, P117