A Facile Sonochemical Method for Synthesis of Mercury Selenide Nanostructures

被引：12

作者：

Esmaeili-Zare, Mahdiyeh ^{[1
]}

Salavati-Niasari, Masoud ^{[1
]}

Ghanbari, Davood ^{[2
]}

Aminifazl, Alireza ^{[3
]}

机构：

[1] Univ Kashan, Inst Nano Sci & Nano Technol, Kashan, Iran

[2] Islamic Azad Univ, Arak Branch, Young Researchers Club, Arak, Iran

[3] Inst Color Sci & Technol, Tehran, Iran

来源：

JOURNAL OF CLUSTER SCIENCE | 2013年 / 24卷 / 03期

关键词：

Complex precursor; HgSe; Sonochemical synthesis; Nanoparticle; HYDROTHERMAL PROCESS; NANOPARTICLES; NANOCRYSTALS; DEPOSITION; CONVERSION; COMPLEXES; NANORODS; GROWTH; ROUTE; FILMS;

D O I：

10.1007/s10876-013-0585-0

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Mercury selenide (HgSe) nanostructures has been achieved from N-N'-bis(salicylaldehyde)-1,2-phenylenediimino mercury [Hg(salophen)] as a new precursor. Cubic phase HgSe nanoparticles with the size of mostly 20-40 nm were produced by sonication of the Hg(salophen) precursor. The products were characterized by X-ray diffraction, transmission electron microscopy, scanning electron microscopy, photoluminescence, energy dispersive X-ray spectroscopy and Fourier transformed infrared spectroscopy. The results of this paper show that the shape and size of mercury selenide nanostructures can be controlled systematically by adjusting reaction parameters, such as the ultrasonic power, temperature, capping agent and reaction time.

引用

页码：881 / 890

页数：10

共 24 条

[1]

[Anonymous], CHEM ANAL INTRO XRAY

[2]

Broerman J. G., 1969, PHYS REV, V183, P54

[3] Simple sonochemical synthesis and characterization of HgSe nanoparticles [J].