Characterization of Hydrazinium 3,5-Dinitroamine-1,2,4-triazole

被引：3

作者：

Cui, Kejian ^{[1
]}

Meng, Zihui ^{[1
]}

Xu, Zhibin ^{[1
]}

Xue, Min ^{[1
]}

Lin, Zhihui ^{[2
]}

Wang, Bozhou ^{[2
]}

Ge, Zhongxue ^{[2
]}

Qin, Guangmin ^{[2
]}

机构：

[1] Beijing Inst Technol, Sch Chem Engn & Environm, Beijing 100081, Peoples R China

[2] Xian Modern Chem Res Inst, Xian, Peoples R China

来源：

JOURNAL OF ENERGETIC MATERIALS | 2014年 / 32卷

关键词：

energetic material; hydrazinium 3,5-dinitroamine-1,2,4-triazole; triazole; characterization; DERIVATIVES; CHEMISTRY;

D O I：

10.1080/07370652.2013.828246

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

The structure of hydrazinium 3,5-dinitroamine-1,2,4-triazole (HDNAT) was investigated with infrared (IR), mass spectrometry, C-13-NMR, scanning electron microscopy (SEM), and X-ray crystallography. The crystal density of HDNAT was determined as 1.91g/cm(3) using X-ray diffraction. The crystal belongs to a monoclinic system with the space group P2(1). The thermal decomposition process of HDNAT was investigated via thermogravimetry-differential thermal analysis (TG-DTA) at a heating rate of 10K/min and differential scanning calorimetry (DSC) under nonisothermal conditions. The decomposition kinetic and thermodynamic parameters were obtained by the Kissinger and Ozawa method. HDNAT can be analyzed by using a C18 high-performance liquid chromatography (HPLC) column with water : acetonitrile : trifluoroacetic acid (97/3/0.1, v/v/v) as the mobile phase and a capacity factor of 1.33.

引用

页码：S60 / S70

页数：11

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