The Synthesis of Novel Material 2,3-Dimethyl-2,3-dihydrofuro[3,4-b][1,4]dioxine-5,7-dicarboxylic acid

被引：0

作者：

Wang Liping ^{[1
]}

Deng Diandian ^{[1
]}

Yan Hewei ^{[1
]}

Sun Xiaoxia ^{[1
]}

Wei Chaochao ^{[1
]}

机构：

[1] Jiangxi Sci & Technol Normal Univ, Jiangxi Key Lab Organ Chem, Nanchang 330013, Peoples R China

来源：

PROCEEDINGS OF THE 2016 INTERNATIONAL FORUM ON ENERGY, ENVIRONMENT AND SUSTAINABLE DEVELOPMENT (IFEESD) | 2016年 / 75卷

关键词：

2,3-dimethyl-2,3-dihydrofuro[3,4-b][1,4]dioxine-5,7-dicarboxylic acid; organic light-emmitting material; synthesis; pi-conjugated polymers; CONJUGATED POLYMERS; SELENOPHENE;

D O I：

暂无

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 ; 0830 ;

摘要：

A new synthetic approach to synthesize 2,3-dimethyl -2,3-dihydrofuro [3,4-b][1,4]dioxine-5,7 -dicarboxylic acid from a common precursor diglycolic acid was reported. Starting from the commercial material diethylene glycol, diethyl oxalate and 2,3-dibromobutane, the compound was synthesized through oxidation reaction, acylation, hydrolysis and elimination reaction with moderate yield via a five-step reaction. The procedure was described herein with several advantages, including high product yields and easy purification.

引用

页码：776 / 779

页数：4

共 35 条

[31] New wide-bandgap D-A polymer based on pyrrolo [3,4-b] dithieno[2,3-f:3′,2′-h]quinoxalindione and thiazole functionalized benzo[1,2-b:4,5-b′] dithiophene units for high-performance ternary organic solar cells with over 16% efficiency
Keshtov, M. L.
Konstantinov, I. O.
Kuklin, S. A.
Davydova, N. K.
Alekseev, V. G.
Xie, Z.
Agrawal, Anupam
Sharma, Ganesh D.
SUSTAINABLE ENERGY & FUELS, 2022, 6 (03) : 682 - 692
[32] Screening, synthesis, crystal structure, and molecular basis of 6-amino-4-phenyl-1,4-dihydropyrano[2,3-c]pyrazole-5-carbonitriles as novel AKR1C3 inhibitors
Zheng, Xuehua
Jiang, Zan
Li, Xiaolin
Zhang, Chen
Li, Zhe
Wu, Yinuo
Wang, Xinhua
Zhang, Chao
Luo, Hai-bin
Xu, Jun
Wu, Deyan
BIOORGANIC & MEDICINAL CHEMISTRY, 2018, 26 (22) : 5934 - 5943
[33] Synthesis and analgesic activity of some novel 2-substituted 1,3,4-thiadiazolo[2,3-b] disubstituted/tetrasubstituted thieno[3,2-e] pyrimidin-5(4H)-ones
Prasad, MR
Pathak, US
Rao, ARR
ARZNEIMITTEL-FORSCHUNG-DRUG RESEARCH, 2000, 50 (10): : 904 - 909
[34] Synthesis, Crystal Structure and Insecticidal Activities of (4aR,7aS)-6-Benzyl-1-((R)-2-(2-chlorophenyl)-4,5-dihydrothiazole-4-carbonyl)hexahydro-5H-pyrrolo [3,4-b] pyridine-5,7(6H)-dione
Liu Jing-Bo
Qin Na
Wang Yuan-Hong
Li Yu-Xin
Li Zheng-Ming
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2021, 40 (05) : 659 - 665
[35] Synthesis, Crystal Structure and Insecticidal Activities of(4aR,7aS)-6-Benzyl-1-((R)-2-(2-chlorophenyl)-4,5-dihydrothiazole-4-carbonyl)hexahydro-5H-pyrrolo[3,4-b]pyridine-5,7(6H)-dione
刘敬波
秦娜
王远宏
李玉新
李正名
Chinese Journal of Structural Chemistry, 2021, 40 (05) : 659 - 665

← 1 2 3 4 →