Ultrasonic synthesis of two new zinc(II) bipyridine coordination polymers: New precursors for preparation of zinc(II) oxide nano-particles

被引：42

作者：

Fard, Mohammad Jaafar Soltanian ^{[1
]}

Hayati, Payam ^{[2
]}

Firoozadeh, Azita ^{[1
]}

Janczak, Jan ^{[3
]}

机构：

[1] Islamic Azad Univ, Fac Chem Sci, Firoozabad Branch, Dept Chem, POB 74715-117, Firoozabad, Fars, Iran

[2] Islamic Azad Univ, Dashtestan Branch, Dept Chem, Borazjan, Iran

[3] Polish Acad Sci, Inst Low Temp & Struct Res, POB 1410 Okolna 2 Str, PL-50950 Wroclaw, Poland

来源：

ULTRASONICS SONOCHEMISTRY | 2017年 / 35卷

关键词：

Nanoparticles; Zinc(II) oxides; Coordination polymer; Ultrasonic; Crystal; ZNO THIN-FILMS; STRUCTURAL-CHARACTERIZATION; SONOCHEMICAL SYNTHESIS; LEAD(II) OXIDE; COUNTER-ION; NANOPARTICLES; SUPRAMOLECULE; LIGAND; GROWTH; PBO;

D O I：

10.1016/j.ultsonch.2016.11.009

中图分类号：

O42 [声学];

学科分类号：

070206 ; 082403 ;

摘要：

Nanoparticles of two zinc(II) coordination polymers (CPs), [Zn(mu-4,4'-bipy)Cl-2](n) (1) and [Zn(mu-4,4'-bipy)Br-2](n), (2) L = bpy = 4,4'-bipyridine ligand, have been synthesized by use of a sonochemical process and characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRPD), Fourier transform infrared spectroscopy (FTIR) spectroscopy and elemental analyses. The single crystal X-ray data of compounds 1 and 2 imply that the Zn+2 ions are four coordinated. Topological analysis shows that 1D coordination networks of 1 and 2 can be classified as underlying nets of topological types 2C1. Nanoparticles of zinc(II) oxide have been prepared by calcination of two different zinc (II) CPs at 450 degrees C that were characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRD) and IR spectroscopy. (C) 2016 Elsevier B.V. All rights reserved.

引用

页码：502 / 513

页数：12

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