A NEW METHOD OF CURING EPOXY RESIN BY USING BIS(HEPTAPHENYLALUMINOSILSESQUIOXANE) AS A HARDENER

被引:0
作者
Chmielewska, Danuta [1 ]
Barczewski, Mateusz [1 ]
Sterzynski, Tomasz [1 ]
机构
[1] Politechn Poznanska, Inst Technol Mat, PL-61138 Poznan, Poland
关键词
epoxy resin; POSS; thermal analysis; crosslinking; THERMOMECHANICAL PROPERTIES; THERMAL-PROPERTIES; POSS; MORPHOLOGY; SILSESQUIOXANE; NANOCOMPOSITES; COMPOSITES;
D O I
暂无
中图分类号
O63 [高分子化学(高聚物)];
学科分类号
070305 ; 080501 ; 081704 ;
摘要
The curing process of epoxy resin Epidian 6 with bis(heptaphenylaluminosilsesquioxane) was studied. The curing conditions for the defined compositions were established on the basis of measurements made during the crosslinking reaction. Differential scanning calorimetry (DSC) was used to determine the temperature of the exothermal reaction related to the course of the curing process. Also, the temperature of crosslinking process and gel time at ambient temperature were determined. The homogeneity of the distribution of FOSS additives in the epoxy matrix was investigated using microscopic analysis (SEM). Fourier transform infrared (FT-IR) spectroscopy was used to evaluate the chemical changes in the resin. It was shown that bis(heptaphenylaluminosilsesquioxane) can be applied as a curing agent for epoxy resins, with the main advantages of a low curing temperature and long life time.
引用
收藏
页码:270 / 275
页数:6
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