Biosynthesis of Au nanoparticles using olive leaf extract

被引:207
|
作者
Khalil, Mostafa M. H. [1 ]
Ismail, Eman H. [1 ]
El-Magdoub, Fatma [1 ]
机构
[1] Ain Shams Univ, Fac Sci, Dept Chem, Cairo, Egypt
关键词
Biosynthesis; Gold nanoparticles; Olive leaf extract; Antioxidant; HIGH-YIELD SYNTHESIS; GOLD NANOPARTICLES; GREEN SYNTHESIS; ANTIMICROBIAL ACTIVITY; BIOLOGICAL SYNTHESIS; PHENOLIC-COMPOUNDS; SILVER; ANTIOXIDANT; SIZE; IDENTIFICATION;
D O I
10.1016/j.arabjc.2010.11.011
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The biological synthesis of gold nanoparticles (AuNPs) of various shapes (triangle, hexagonal, and spherical) using hot water olive leaf extracts as reducing agent is reported. The size and the shape of Au nanoparticles are modulated by varying the ratio of metal salt and extract in the reaction medium. Only 20 min were required for the conversion into gold nanoparticles at room temperature, suggesting a reaction rate higher or comparable to those of nanoparticles synthesis by chemical methods. The variation of the pH of the reaction medium gives AuNPs nanoparticles of different shapes. The nanoparticles obtained are characterized by UV-Vis spectroscopy, photoluminescence, transmission electron microscopy (TEM), X-ray diffraction (XRD), FTIR spectroscopy and thermogravimetric analysis. The TEM images showed that a mixture of shapes (triangular, hexagonal and spherical) structures was formed at lower leaf broth concentration and high pH, while smaller spherical shapes were obtained at higher leaf broth concentration and low pH. (C) 2010 King Saud University. Production and hosting by Elsevier B. V. All rights reserved.
引用
收藏
页码:431 / 437
页数:7
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