Preparation of nanocrystalline ferroelectric BaBi4Ti4O15 by Pechini method

被引:30
作者
Murugan, AV
Navale, SC
Ravi, V [1 ]
机构
[1] Natl Chem Lab, Phys & Mat Chem Div, Pune 411008, Maharashtra, India
[2] Govt India, C MET, Dept Informat Technol, Pune 411008, Maharashtra, India
关键词
powders chemical preparation; electron microscopy; dielectric properties; ferroelectric properties;
D O I
10.1016/j.matlet.2005.10.068
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A gel was formed when an aqueous solution of BaCl2, BiNO3, TiOCl2 and citric acid in stoichiometric ratio is heated on a water bath. This gel on decomposition at 600 degrees C produced the nano crystallites of ternary oxide, BaBi4Ti4O15 (BBT). The phase contents and lattice parameters were Studied by the powder X-ray diffraction (XRD). Particle size and morphology was studied by transmission electron spectroscopy (TEM). The room temperature dielectric constant at I KHz is 90. The ferroelectric hysteresis loop parameters of these samples were also studied by a home built Sawyer-tower circuit. (c) 2005 Elsevier B.V. All rights reserved.
引用
收藏
页码:1023 / 1025
页数:3
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