Simultaneously Enhancing Spectral Resolution and Sensitivity in Heteronuclear Correlation NMR Spectroscopy

被引：134

作者：

Paudel, Liladhar ^{[1
]}

Adams, Ralph W. ^{[1
]}

Kiraly, Peter ^{[1
,2
]}

Aguilar, Juan A. ^{[1
,3
]}

Foroozandeh, Mohammadali ^{[1
]}

Cliff, Matthew J. ^{[4
]}

Nilsson, Mathias ^{[1
,5
]}

Sandor, Peter ^{[6
]}

Waltho, Jonathan P. ^{[4
]}

Morris, Gareth A. ^{[1
]}

机构：

[1] Univ Manchester, Sch Chem, Manchester M13 9PL, Lancs, England

[2] Hungarian Acad Sci, Inst Organ Chem, H-1025 Budapest, Hungary

[3] Univ Durham, Dept Chem, Durham DH1 3LE, England

[4] Manchester Inst Biotechnol, Manchester M1 7DN, Lancs, England

[5] Univ Copenhagen, Dept Food Sci, DK-1958 Frederiksberg C, Denmark

[6] Agilent Technol R&D, D-76337 Waldbronn, Germany

来源：

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION | 2013年 / 52卷 / 44期

基金：

英国生物技术与生命科学研究理事会; 英国工程与自然科学研究理事会;

关键词：

bilinear rotation decoupling; gHSQC; homonuclear decoupling; NMR spectroscopy; structure elucidation; BAND INVERSION; HOMONUCLEAR; PULSES;

D O I：

10.1002/anie.201305709

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

BIRD's eye view: Adding periodic BIRD J-refocusing (BIRD=bilinear rotation decoupling) to data acquisition in an HSQC experiment causes broadband homonuclear decoupling, giving a single signal for each proton chemical shift. This pure shift method improves both resolution and signal-to-noise ratio, without the need for special data processing. © 2013 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the Creative Commons Attribution License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited.

引用

页码：11616 / 11619

页数：4

共 50 条

[21] SCREENES: Enhancing non-uniform sampling reconstruction for symmetrical NMR spectroscopy
Fang, Ze
Chen, Bo
Huang, Chengda
Yuan, Yifei
Luo, Yao
Wu, Liubin
Chen, Yida
Huang, Yuqing
Yang, Yu
Lin, Enping
Chen, Zhong
ANALYTICA CHIMICA ACTA, 2024, 1303
[22] Heteronuclear multidimensional NMR spectroscopy of solubilized membrane proteins: Resonance assignment of native bacteriorhodopsin
Schubert, M
Kolbe, M
Kessler, B
Oesterhelt, D
Schmieder, P
CHEMBIOCHEM, 2002, 3 (10) : 1019 - 1023
[23] Next-Generation Heteronuclear Decoupling for High-Field Biomolecular NMR Spectroscopy**
Schilling, Franz
Warner, Lisa R.
Gershenzon, Naum I.
Skinner, Thomas E.
Sattler, Michael
Glaser, Steffen J.
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2014, 53 (17) : 4475 - 4479
[24] Full Sensitivity and Enhanced Resolution in Homodecoupled Band-Selective NMR Experiments
Castanar, Laura
Nolis, Pau
Virgili, Albert
Parella, Teodor
CHEMISTRY-A EUROPEAN JOURNAL, 2013, 19 (51) : 17283 - 17286
[25] Recent advances in high-resolution solid-state NMR spectroscopy
Schwalbe, H
Bielecki, A
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2001, 40 (11) : 2045 - 2050
[26] Facing and Overcoming Sensitivity Challenges in Biomolecular NMR Spectroscopy
Ardenkjaer-Larsen, Jan-Henrik
Boebinger, Gregory S.
Comment, Arnaud
Duckett, Simon
Edison, Arthur S.
Engelke, Frank
Griesinger, Christian
Griffin, Robert G.
Hilty, Christian
Maeda, Hidaeki
Parigi, Giacomo
Prisner, Thomas
Ravera, Enrico
van Bentum, Jan
Vega, Shimon
Webb, Andrew
Luchinat, Claudio
Schwalbe, Harald
Frydman, Lucio
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2015, 54 (32) : 9162 - 9185
[27] Orchestrated approaches using pure shift NMR: Extraction of spectral parameters, ultra-high resolution, and sensitivity enhancement
Mishra, Sandeep Kumar
Suryaprakash, N.
MAGNETIC RESONANCE IN CHEMISTRY, 2018, 56 (10) : 893 - 909
[28] High-resolution NMR spectroscopy in inhomogeneous fields
Chen, Zhong
Cai, Shuhui
Huang, Yuqing
Lin, Yulan
PROGRESS IN NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY, 2015, 90-91 : 1 - 31
[29] Sensitivity enhancement in transverse relaxation optimized NMR spectroscopy
Zhu, GA
Kong, XM
Yan, XZ
Sze, KH
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1998, 37 (20) : 2859 - 2861
[30] Mobile sensor for high resolution NMR spectroscopy and imaging
Danieli, Ernesto
Mauler, Joerg
Perlo, Juan
Bluemich, Bernhard
Casanova, Federico
JOURNAL OF MAGNETIC RESONANCE, 2009, 198 (01) : 80 - 87

← 1 2 3 4 5 →