Optimization and characterization of 1,8-cineole/hydroxypropyl-β-cyclodextrin inclusion complex and study of its release kinetics

被引：65
作者：
Yin, Hao [1 ]
Wang, Chenxiao [1 ]
Yue, Jin [1 ]
Deng, Yun [1 ]
Jiao, Shunshan [1 ]
Zhao, Yanyun [2 ]
Zhou, Jie [3 ]
Cao, Ting [3 ]
机构：
[1] Shanghai Jiao Tong Univ, Bor S Luh Food Safety Res Ctr, SJTU OSU Innovat Ctr Environm Sustainabil, Key Lab Urban Agr,Minist Agr, Shanghai 200240, Peoples R China
[2] Oregon State Univ, Dept Food Sci & Technol, 100 Wiegand Hall, Corvallis, OR 97331 USA
[3] Sichuan Chenyu Forestry Dev Co Ltd, Yibin 644000, Peoples R China
来源：
FOOD HYDROCOLLOIDS | 2021年 / 110卷
基金：
中国国家自然科学基金;
关键词：
1,8-Cineole; Hydroxypropyl-beta-cyclodextrin; Inclusion complex; Release kinetics; HYDROXYPROPYL-BETA-CYCLODEXTRIN; ESSENTIAL OIL; ENCAPSULATION; 1,8-CINEOLE; STABILITY; SOLUBILITY; LEAVES; RATS;
D O I：
10.1016/j.foodhyd.2020.106159
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
Essential oils can be capsulated by cyclodextrin to enhance its thermal stability and preserve the bioactivity. In this study, 1,8-cineole was used as a guest molecule to prepare the cyclodextrin inclusion complexes (ICs). The formulation and processing parameters were optimized using the response surface methodology (RSM), and the optimal conditions were identified to be: 2.30 h of encapsulating time, 30.1 degrees C of encapsulating temperature and 0.99 of molar ratio of 1,8-cineole to HP-beta-CD. The corresponding encapsulation efficiency and loading efficiency were 83.17% and 8.40%, respectively. The produced 1,8-cineole/HP-beta-CD ICs was characterized by SEM, FTIR and TGA, and the results proved the enhanced thermal stability of IC. The release behavior and kinetics of IC was investigated and showed that at elevated temperature and relative humidity, the releasing rate of 1,8-cineole from the ICs increased and followed the Fick's law.
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页数：10
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