Accuracy assessment of elastic strain measurement by EBSD

被引:99
作者
Villert, S. [1 ,2 ]
Maurice, C. [1 ]
Wyon, C. [2 ]
Fortunier, R. [1 ]
机构
[1] Ecole Natl Super Mines, Ctr SMS, UMR 5146, CNRS, F-42023 St Etienne 2, France
[2] CEA LETI, F-38054 Grenoble 9, France
关键词
EBSD pattern simulation; elastic strain measurement; electron backscatter diffraction; finite element; four-point bending; SiGe layer; ELECTRON BACKSCATTER DIFFRACTION; PATTERNS; DEFECTS;
D O I
10.1111/j.1365-2818.2009.03120.x
中图分类号
TH742 [显微镜];
学科分类号
摘要
A detailed accuracy analysis of electron backscatter diffraction (EBSD) elastic strain measurement has been carried out using both simulated and experimental patterns. Strains are determined by measuring shifts between two EBSD patterns (one being the reference) over regions of interest (ROI) using an iterative cross-correlation algorithm. An original minimization procedure over 20 regions of interests gives a unique solution for the eight independent components of the deviatoric displacement gradient tensor. It is shown that this method leads to strain measurements on simulated patterns with an accuracy better than 10(-4). The influence of the projection parameters is also investigated. The accuracy assessment is illustrated by two worked examples: (i) four-point bending of a silicon single crystal and (ii) Si1 - xGex layers on a Si substrate. Experimental results are compared with finite-element simulations.
引用
收藏
页码:290 / 301
页数:12
相关论文
共 16 条
[1]   Improved approaches to the determination of residual stresses in micro regions with the KOSSEL and the XRT technique [J].
Bauch, J ;
Wege, S ;
Böhling, M ;
Ullrich, HJ .
CRYSTAL RESEARCH AND TECHNOLOGY, 2004, 39 (07) :623-633
[2]   Digital image correlation used to analyze the multiaxial behavior of rubber-like materials [J].
Chevalier, L ;
Calloch, S ;
Hild, F ;
Marco, Y .
EUROPEAN JOURNAL OF MECHANICS A-SOLIDS, 2001, 20 (02) :169-187
[3]  
DAY A, 1993, THESIS U BRISTOL UK
[4]   Spherical EBSD [J].
Day, A. P. .
JOURNAL OF MICROSCOPY, 2008, 230 (03) :472-486
[5]   Progressive steps in the development of electron backscatter diffraction and orientation imaging microscopy [J].
Dingley, D .
JOURNAL OF MICROSCOPY-OXFORD, 2004, 213 :214-224
[6]   Strain field in silicon on insulator lines using high resolution x-ray diffraction [J].
Gailhanou, M. ;
Loubens, A. ;
Micha, J. -S. ;
Charlet, B. ;
Minkevich, A. A. ;
Fortunier, R. ;
Thomas, O. .
APPLIED PHYSICS LETTERS, 2007, 90 (11)
[7]  
Guyon F., 2000, 04199 INSA ROUEN
[8]  
Lassen NCK, 1999, J MICROSC-OXFORD, V195, P204, DOI 10.1046/j.1365-2818.1999.00581.x
[9]   An algorithm for refinement of lattice parameters using CBED patterns [J].
Morawiec, A. .
ULTRAMICROSCOPY, 2007, 107 (4-5) :390-395
[10]  
ROMAINLATU E, 2006, THESIS I NATL POLYTE