Synthesis and NMR Spectral Studies of the 7-C60-Adduct of N,N-(Tetrachlorophthaloyl)dehydroabietylamine

被引：2
作者：
Zhou, Zhi [1 ,2 ]
Lin, Zhongxiang [1 ]
机构：
[1] Nanjing Forestry Univ, Coll Chem Engn, Nanjing 210037, Jiangsu, Peoples R China
[2] Kaili Univ, Coll Life & Environm Sci, Kaili 556011, Guizhou, Peoples R China
来源：
MOLECULES | 2012年 / 17卷 / 04期
基金：
中国国家自然科学基金;
关键词：
7-C-60-adduct of N; N-(tetrachlorophthaloyl)dehydroabietylamine; H-1-NMR; C-13-NMR; 2D NMR; C-1 symmetric structure; 2-SUBSTITUTED 1,4-BENZODIOXANES; DERIVATIVES; RESOLUTION;
D O I：
10.3390/molecules17044209
中图分类号：
Q5 [生物化学]; Q7 [分子生物学];
学科分类号：
071010 ; 081704 ;
摘要：
The 7-C-60-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine was synthesized for the first time and characterized by IR, UV-vis, mass and NMR spectral studies. The H-1-NMR and C-13-NMR resonance signals of the new compound are unambiguously assigned by using homo-and heteronuclear 2D NMR spectroscopic techniques such as COSY, ROESY, HSQC and HMBC. The C-1 symmetric structure with 6,6-junction of compound was determined.
引用
收藏
页码：4209 / 4218
页数：10
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