Rapid Synthesis of Alkyloxy Porphyrins Under Microwave Irradiation

被引：3

作者：

Ren, Qing-Gang ^{[1
]}

Fang, Yan-Xiong ^{[1
]}

Ji, Hong-Bing ^{[2
]}

Wei, Xing-Chuan ^{[3
]}

Deng, Yun-Quan ^{[1
]}

Zhang, Kun ^{[1
]}

机构：

[1] Guangdong Univ Technol, Fac Chem Engn & Light Ind, Guangzhou 510006, Guangdong, Peoples R China

[2] Sun Yat Sen Univ, Sch Chem & Chem Engn, Guangzhou 510275, Guangdong, Peoples R China

[3] Guangzhou Univ, Fac Chem & Chem Engn, Guangzhou, Guangdong, Peoples R China

来源：

SYNTHETIC COMMUNICATIONS | 2009年 / 39卷 / 01期

基金：

中国国家自然科学基金;

关键词：

Alkyl halide; alkyloxy porphyrin; ether; microwave; Williamson; MESO-TETRAPHENYLPORPHYRIN CHLORIDE; SELECTIVE OXIDATION; COUPLING REACTIONS; WATER;

D O I：

10.1080/00397910802369505

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Alkyloxy porphyrins have been prepared by direct coupling of 5-para-hydroxyphenyl-10,15,20-triphenylporphyrin and alkyl halides under microwave irradiation within several minutes. The length of the alkyl halides has no obvious effect on the yields and reaction time; however, the steric structure of the alkyl halides has a great impact on the reaction time. All the products were confirmed by H-1 NMR.

引用

页码：20 / 28

页数：9

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