Rapid Synthesis of Alkyloxy Porphyrins Under Microwave Irradiation

被引：3
|
作者：
Ren, Qing-Gang [1 ]
Fang, Yan-Xiong [1 ]
Ji, Hong-Bing [2 ]
Wei, Xing-Chuan [3 ]
Deng, Yun-Quan [1 ]
Zhang, Kun [1 ]
机构：
[1] Guangdong Univ Technol, Fac Chem Engn & Light Ind, Guangzhou 510006, Guangdong, Peoples R China
[2] Sun Yat Sen Univ, Sch Chem & Chem Engn, Guangzhou 510275, Guangdong, Peoples R China
[3] Guangzhou Univ, Fac Chem & Chem Engn, Guangzhou, Guangdong, Peoples R China
来源：
SYNTHETIC COMMUNICATIONS | 2009年 / 39卷 / 01期
基金：
中国国家自然科学基金;
关键词：
Alkyl halide; alkyloxy porphyrin; ether; microwave; Williamson; MESO-TETRAPHENYLPORPHYRIN CHLORIDE; SELECTIVE OXIDATION; COUPLING REACTIONS; WATER;
D O I：
10.1080/00397910802369505
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Alkyloxy porphyrins have been prepared by direct coupling of 5-para-hydroxyphenyl-10,15,20-triphenylporphyrin and alkyl halides under microwave irradiation within several minutes. The length of the alkyl halides has no obvious effect on the yields and reaction time; however, the steric structure of the alkyl halides has a great impact on the reaction time. All the products were confirmed by H-1 NMR.
引用
收藏
页码：20 / 28
页数：9
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