Synthesis and crystal structure of 2-((1-phenyl-3-(thiophen-2-yl)-1H-pyrazol-4-yl)methylene)-2,3-dihydro-1H-inden-1-one, C23H16N2OS

被引：0
作者：
Alqahtani, Alaa [3 ]
Abdel-Wahab, Bakr F. [4 ,5 ]
Hegazy, Amany S. [1 ]
Kariuki, Benson M. [1 ]
El-Hiti, Gamal A. [2 ]
机构：
[1] Cardiff Univ, Sch Chem, Main Bldg,Pk Pl, Cardiff CF10 3AT, S Glam, Wales
[2] King Saud Univ, Coll Appl Med Sci, Dept Optometry, POB 10219, Riyadh 11433, Saudi Arabia
[3] Umm Al Qura Univ, Coll Pharm, Pharmaceut Chem Dept, Mecca, Saudi Arabia
[4] Shaqra Univ, Coll Sci & Humanities, Dept Chem, Duwadimi, Saudi Arabia
[5] Natl Res Ctr, Appl Organ Chem Dept, Giza, Egypt
来源：
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2019年 / 234卷 / 05期
关键词：
EFFICIENT SYNTHESIS; PYRAZOLE;
D O I：
10.1515/ncrs-2019-0189
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
C23H16N2OS, orthorhombic, Pna2(1) (no. 33), a =19.4988(9) angstrom, b =19.5060(9) angstrom, c = 9.2893(4) angstrom, V=3533.1(3) angstrom(3), z= 8, R-gt (F) = 0.0501, wR(ref)(F-2) = 0.1269, T = 296(2) K.
引用
收藏
页码：969 / 971
页数：3
相关论文
共 50 条
  • [21] Synthesis,Crystal Structure and Biological Activity of 2-Chloro-5-(((5-(1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-yl)-4-phenyl-4H-1,2,4-triazol-3-yl)thio)methyl)thiazole
    沈钟华
    翟志文
    孙召慧
    翁建全
    谭成侠
    刘幸海
    [J]. 结构化学, 2017, 36 (07) : 1137 - 1141
  • [22] Synthesis, Crystal Structure and Biological Activity of 2-Chloro-5-(((5-(1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-yl)-4-phenyl-4H-1,2,4-triazol-3-yl)thio)methyl)thiazole
    Shen Zhong-Hua
    Zhai Zhi-Wen
    Sun Zhao-Hui
    Weng Jian-Quan
    Tan Cheng-Xia
    Liu Xing-Hai
    [J]. CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2017, 36 (07) : 1137 - 1141
  • [23] Design, Synthesis, Molecular Docking, and Anti-inflammatory Activity of 2-[(E)-{1-[4-(4-Chlorophenyl)-1,3-thiazol-2-yl]-1H-pyrazol-4-yl}(hydroxyimino)methyl]phenol and {1-[4-(4-Chlorophenyl)-1,3-thiazol-2-yl]-1H-pyrazol-4-yl}(2-hydroxyphenyl)methanone Derivatives
    Darekar, N. R.
    Takate, S. J.
    Akolkar, H. N.
    Shaikh, M. H.
    Khedkar, V. M.
    Raut, D. N.
    Mhaske, S. D.
    [J]. RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2024, 60 (09) : 1818 - 1827
  • [24] Microwave-assisted synthesis of 1-{2-[(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy]phenyl}-3-(3-aryl-1-phenyl-1H-pyrazol-4-yl)prop-2-en-1-ones and their antimicrobial activity
    Ashok, D.
    Padmavati, K.
    [J]. RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2016, 86 (04) : 907 - 914
  • [25] Microwave-assisted synthesis of 1-{2-[(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy]phenyl}-3-(3-aryl-1-phenyl-1H-pyrazol-4-yl)prop-2-en-1-ones and their antimicrobial activity
    D. Ashok
    K. Padmavati
    [J]. Russian Journal of General Chemistry, 2016, 86 : 907 - 914
  • [26] 2-Bromo-1-(1H-pyrazol-4-yl)ethanone: versatile precursors for novel mono-, bis- and poly{6-(1H-pyrazol-4-yl)-[1,2,4]triazolo [3,4-b][1,3,4]thiadiazines}
    Salem, Mostafa E.
    Darweesh, Ahmed F.
    Farag, Ahmad M.
    Elwahy, Ahmed H. M.
    [J]. TETRAHEDRON, 2016, 72 (05) : 712 - 719
  • [27] Efficient Multicomponent Synthesis of Methyl 2-(Benzyloxy)-5-[2-(2-{[3-(substituted phenyl)-1-phenyl-1H-pyrazol-4-yl]­methylidene}hydrazinyl)-1,3-thiazol-4-yl]benzoates
    V. R. Bhosale
    V. S. Kapase
    [J]. Russian Journal of Organic Chemistry, 2025, 61 (1) : 105 - 110
  • [28] Antimicrobial and computational investigation of two 2,3-dihydro-1H-inden-1-one derived fluorinated chalcone motifs
    Shinde, Rahul Ashok
    Adole, Vishnu Ashok
    Jagdale, Bapu Sonu
    [J]. VIETNAM JOURNAL OF CHEMISTRY, 2021, 59 (06) : 800 - 812
  • [29] Crystal structure of 3-{5-[3-(4-fluorophenyl)-1-isopropyl-1H-indol-2-yl]-1H-pyrazol-1-yl}indolin-2-one ethanol monosolvate
    Rahman, Md. Lutfor
    Kulkarni, Ajaykumar D.
    Yusoff, Mashitah Mohd.
    Kwong, Huey Chong
    Quah, Ching Kheng
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2016, 72 : 283 - +
  • [30] Straightforward and Clean Ultrasound-Promoted Synthesis of 2-(4,5-Dihydro-1H-pyrazol-1-yl) pyrimidines
    Kuhn, Bruna P.
    Malavolta, Juliana L.
    Casagrande, Gleison A.
    Raminelli, Cristiano
    Quina, Frank H.
    Pereira, Claudio M. P.
    Flores, Alex F. C.
    Pizzuti, Lucas
    [J]. JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, 2015, 26 (06) : 1306 - 1312
12345