Experimental Investigation and Comparative Study of Sintering of Microcrystalline Nickel Using Microwave and Conventional Method

被引:3
作者
Hussain, Md Izhar [1 ]
Hussain, Manowar [2 ]
Gupta, Ankit [3 ]
Ahmad, Gulshad Nawaz [4 ]
机构
[1] OP Jindal Univ, Dept Met Engn, Raigarh 496109, Chhattisgarh, India
[2] Chaitanya Bharathi Inst Technol, Dept Mech Engn, Hyderabad 500075, Telangana, India
[3] Tennessee Technol Univ, Dept Mech Engn, Cookeville, TN 38505 USA
[4] Tennessee Technol Univ, Ctr Mfg Res, Cookeville, TN 38505 USA
关键词
Mass transport; Microwave sintering; Microcrystalline nickel; Densification; Shrinkage; Conventional sintering;
D O I
10.1007/s13369-021-05510-0
中图分类号
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号
07 ; 0710 ; 09 ;
摘要
The present work has been conducted to investigate and compare the mass transport mechanism of Ni-powder particles in conventional and microwave sintering process. The linear shrinkage method was used to investigate the mass transport mechanism on the basis of estimated sintering exponent (n) at different temperatures. Both types of sintering were carried out at various temperatures, and the results revealed that microwave sintering provides better results of densification and shrinkage as compared to conventional sintering. Field emission scanning electron microscopy (FESEM) and energy-dispersive X-ray spectroscopy (EDX) analysis were carried out for the characterization of Ni-powder for microstructural and elemental analysis. The value of sintering exponent found through linear shrinkage method for conventional was 9.4791, 8.1836, 6.9013, 7.3286, 5.2006 and 4.9531 at 500 degrees C-1000 degrees C, respectively, and microwave sintering was 7.0972, 5.2957,5.2942 and 6.0934 at 500 degrees C-800 degrees C, respectively.
引用
收藏
页码:7757 / 7771
页数:15
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