Study of Hyperthermia Through the Bioplasma Treatment and Magnetic Properties of Fe3O4 Nanoparticles

被引:7
作者
Choi, Hyunkyung [1 ]
Kim, Sam Jin [1 ]
Choi, Eun Ha [2 ]
Kim, Chul Sung [1 ]
机构
[1] Kookmin Univ, Dept Phys, Seoul 136702, South Korea
[2] Kwangwoon Univ, Plasma Biosci Res Ctr, Seoul 139701, South Korea
基金
新加坡国家研究基金会;
关键词
Fe3O4; hyperthermia; Mossbauer spectroscopy; nanoparticle; plasma treatment; MOSSBAUER;
D O I
10.1109/TMAG.2015.2435062
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
Fe3O4 nanoparticles were prepared by the high-temperature thermal decomposition method. Based on the Rietveld refinement, the crystal structure was determined to be a cubic spinel with space group of Pnma. The size and the shape of the nanoparticles were examined using a high-resolution transmission electron microscope (HR-TEM). Also, the Fe3O4 nanoparticles were treated with argon plasma and compared with untreated Fe3O4 nanoparticles. The X-ray diffraction patterns and HR-TEM images show small structural changes. Also, when exposed under Ar plasma, the saturation magnetization of nanoparticles exposed for 30 min was 73.705 emu/g, highest among the samples studied. The self-heating temperature of the sample increases up to 94.6 degrees C after the plasma treatment for 30 min. In addition, Mossbauer measurements were performed with a high external field of 5 T and based on the detailed analysis of the Mossbauer spectra, the spin canting angles in Fe3O4 nanoparticles were determined.
引用
收藏
页数:4
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