Synthesis, Crystal Structure and Fungicidal Activity of 3-(((4-Cyclopropyl-5-Methyl-4H-1,2,4-Triazol-3-yl)Thio)Methyl)Benzonitrile H2O (1:1) Solvent

被引：0

作者：

Jin, Jian-Zhong ^{[1
]}

Sun, Na-Bo ^{[1
]}

机构：

[1] Zhejiang Shuren Univ, Coll Biol & Environm Engn, Hangzhou 310015, Zhejiang, Peoples R China

来源：

JOURNAL OF THE CHEMICAL SOCIETY OF PAKISTAN | 2013年 / 35卷 / 03期

关键词：

1,2,4-triazole; cyclopropane; antifungal activity; synthesis; BIOLOGICAL-ACTIVITIES; 1,2,4-TRIAZOLE DERIVATIVES; DFT CALCULATION; MICROWAVE; BIOACTIVITY;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The title compound (C14H14N4S center dot H2O) were synthesized and recrystallized from ethanol. The compound was characterized by H-1 NMR, elemental analyses and X-ray diffraction. The compound crystallized in the monoclinic space group P2(1)/c with a = 11.289(2), b = 15.675(3), c = 8.4835(17) angstrom, alpha = 90, beta = 104.65(3), gamma = 90 degrees, V = 1452.4(5) angstrom(3), Z = 4 and R = 0.0333 for 2545 observed reflections with I > 2 sigma(I). X-ray analysis reveals that not only intermolecular O-H center dot center dot center dot N interactions. The biological activities results showed that the title compound exhibited significant fungicidal activity towards six test fungi.

引用

页码：955 / 959

页数：5

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