Strontium ferrite powders prepared from oily cold rolling mill sludge by solid-state reaction method

被引:15
作者
Liu, Bo [1 ]
Zang, Shen-Gen [1 ]
Tian, Jian-jun [1 ]
Pan, De-an [1 ]
Zhu, Hang-Xin [1 ]
机构
[1] Univ Sci & Technol Beijing, Adv Mat & Technol Inst, Beijing 100083, Peoples R China
基金
中国国家自然科学基金; 国家高技术研究发展计划(863计划);
关键词
Strontium ferrite powders; Oily cold rolling mill sludge; Solid-state reaction method; Recycling; MAGNETIC-PROPERTIES; BARIUM;
D O I
10.1007/s12598-013-0155-5
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Oily cold rolling mill (CRM) sludge is one of the pollutants emitted by iron and steel plants. Recycling oily CRM sludge can not only reduce pollution but also bring social and environmental benefits. In this study, using oily CRM sludge as sources of iron oxide, the strontium ferrite powders were synthesized in multiple steps including vacuum distillation, magnetic separation, oxidizing roasting, and solidstate reaction. The optimal technological conditions of vacuum distillation and oxidizing roasting were studied carefully. To consider the effects of Fe2O3/SrCO3 mol ratio, calcination temperature, milling time and calcination time on magnetic properties of prepared strontium ferrite powders, the orthogonal experimental method was adopted. The maximum saturation magnetization (62.6 mA center dot m(2)center dot g(-1)) of the synthesized strontium ferrite powders was achieved at the Fe2O3/SrCO3 mol ratio of 6, 5 h milling time, 1250 A degrees C calcination temperature, and 1 h calcination time. Strontium ferrite powders synthesis method not only provides a cheap, high quality raw material for the production of strontium ferrite powders, but also effectively prevents the environmental pollution.
引用
收藏
页码:518 / 523
页数:6
相关论文
共 17 条
  • [1] An overview of utilization of slag and sludge from steel industries
    Das, B.
    Prakash, S.
    Reddy, P. S. R.
    Misra, V. N.
    [J]. RESOURCES CONSERVATION AND RECYCLING, 2007, 50 (01) : 40 - 57
  • [2] Controlling the composition and magnetic properties of strontium hexaferrite synthesized by co-precipitation method
    Hessien, M. M.
    Rashad, M. M.
    El-Barawy, K.
    [J]. JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2008, 320 (3-4) : 336 - 343
  • [3] Synthesis and magnetic properties of strontium hexaferrite from celestite ore
    Hessien, M. M.
    Rashad, M. M.
    Hassan, M. S.
    El-Barawy, K.
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2009, 476 (1-2) : 373 - 378
  • [4] Simple and reproducible preparation of barium hexagonal ferrite by adsorbent combustion method
    Huang, Xiaogu
    Zhang, Jing
    Wang, Lixi
    Zhang, Qitu
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2012, 540 : 137 - 140
  • [5] The effect of SiO2 addition on structural, magnetic and electrical properties of strontium hexa-ferrites
    Hussain, Shahid
    Anis-ur-Rehman, M.
    Maqsood, A.
    Awan, M. S.
    [J]. JOURNAL OF CRYSTAL GROWTH, 2006, 297 (02) : 403 - 410
  • [6] Influence of the iron content on the formation process of substituted Co-Nd strontium hexaferrite prepared by the citrate precursor method
    Jacobo, S. E.
    Herme, C.
    Bercoff, P. G.
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2010, 495 (02) : 513 - 515
  • [7] Synthesis and characterization of SrFe12O19 powder obtained by hydrothermal process
    Jean, Malick
    Nachbaur, Virginie
    Bran, Julien
    Le Breton, Jean-Marie
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2010, 496 (1-2) : 306 - 312
  • [8] Magnetic properties of La-Co substituted M-type strontium hexaferrites prepared by polymerizable complex method
    Kikuchi, Takeyuki
    Nakamura, Tatsuya
    Yamasaki, Tohru
    Nakanishi, Makoto
    Fujii, Tatsuo
    Takada, Jun
    Ikeda, Yasunori
    [J]. JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2010, 322 (16) : 2381 - 2385
  • [9] Liu XD, 2009, STUD FUZZ SOFT COMP, V244, P3
  • [10] Reduction characteristics of oily hot rolling mill sludge by direct reduced iron method
    Park, JW
    Ahn, JC
    Song, H
    Park, K
    Shin, H
    Ahn, JS
    [J]. RESOURCES CONSERVATION AND RECYCLING, 2002, 34 (02) : 129 - 140