Determination of 61 organic pollutants in drinking water by solid phase extraction followed by liquid and gas chromatography coupled to tandem mass spectrometry: an analytical strategy for a routine laboratory

被引：6

作者：

Fortuny, Georgina ^{[1
]}

Pineda, Laura ^{[1
]}

Rubies, Antoni ^{[1
]}

Centrich, Francesc ^{[1
]}

Companyo, Ramon ^{[2
]}

机构：

[1] Lab Agencia Salut Publ Barcelona, Area Anal Organ, Serv Quim, Barcelona, Spain

[2] Univ Barcelona, Dept Analyt Chem, Fac Chem, E-08028 Barcelona, Spain

来源：

INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY | 2013年 / 93卷 / 07期

关键词：

polycyclic aromatic hydrocarbons (PAHs); pesticides; polychlorinated biphenyls (PCB); drinking water; solid phase extraction (SPE); liquid chromatography (LC); gas chromatography (GC); mass spectrometry (MS); POLYCYCLIC AROMATIC-HYDROCARBONS; PESTICIDES; MS/MS; MS;

D O I：

10.1080/03067319.2011.649745

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A method for determination of 61 organic pollutants (polycyclic aromatic hydrocarbons and organochlorine, organophosphorous and organonitrogen pesticides) is proposed. It is based on solid phase extraction (SPE) and subsequent analysis of the extract by liquid and gas chromatography coupled to tandem mass spectrometry. Method validation yielded to the following values: limits of quantification, from 0.005 to 0.020 mu gL(1); trueness, 95% to 113% and reproducibility (as percent relative standard deviation), 2% to 15%. Additionally, the method performed well in various proficiency tests.

引用

页码：707 / 726

页数：20

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