Nanocrystalline (Fe60Al40)80Cu20 alloy prepared by mechanical alloying

被引:21
作者
Krifa, M. [1 ]
Mhadhbi, M. [1 ]
Escoda, L. [2 ]
Gueell, M. [2 ]
Sunol, J. J. [2 ]
Llorca-Isern, N. [3 ]
Artieda-Guzman, C. [3 ]
Khitouni, M. [1 ]
机构
[1] Univ Sfax, FSS, Lab Chim Inorgan, UR 12 22 99, Sfax 3018, Tunisia
[2] Univ Girona, Dept Fis, Girona 17071, Spain
[3] Univ Barcelona, Dept CMEM, E-08028 Barcelona, Spain
关键词
Mechanical alloying; Nanostructured materials; Phase transitions; X-ray diffraction; Magnetic properties; Hard ferromagnetic behavior; MAGNETIC-PROPERTIES; IRON ALUMINIDES; BEHAVIOR; NICKEL;
D O I
10.1016/j.jallcom.2012.11.131
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
A nanostructured disordered Fe(Al, Cu) solid solution was obtained from prealloyed FeAl and elemental Cu powders using a high-energy ball mill. The transformations occurring in the material during milling were studied with the use of X-ray diffraction. The transformation of the phase depends upon the milling time. With the increase of milling time all Cu atoms became dissolved in the bcc Fe and the final product of the MA process was the nanocrystalline Fe(Al, Cu) solid solution with a mean crystallite size of 10 nm. Scanning electron microscopy (SEM) was employed to examine the morphology of the samples as a function of milling times. Magnetic properties were also investigated and were related to the microstructural changes. The system showed hard magnetic behavior. (C) 2012 Elsevier B. V. All rights reserved.
引用
收藏
页码:51 / 58
页数:8
相关论文
共 44 条
[1]   Tailoring of paramagnetic (structurally ordered) nanometric grains separated by ferromagnetic (structurally disordered) grain boundaries:: Isolating grain-boundary magnetic effects -: art. no. 052402 [J].
Amils, X ;
Nogués, J ;
Suriñach, S ;
Muñoz, JS ;
Baró, MD ;
Hernando, A ;
Morniroli, JP .
PHYSICAL REVIEW B, 2001, 63 (05)
[2]  
[Anonymous], 1965, PHYS PRINCIPLES MAGN
[3]   Study of the enhancement of the magnetic properties of Fe70Al30 in the order-disorder transition [J].
Apiñaniz, E ;
Plazaola, F ;
Garitaonandia, JS ;
Martín, D ;
Jimenez, JA .
JOURNAL OF APPLIED PHYSICS, 2003, 93 (10) :7649-7651
[4]  
Apinaniz E., 2001, Journal of Non-Crystalline Solids, V287, P302, DOI [10.1016/s0022-3093(01)00570-1, DOI 10.1016/S0022-3093(01)00570-1]
[5]  
Baker I., 1997, P INT S NICK IR AL M, P145
[6]   NANOCRYSTALLINE MATERIALS [J].
BIRRINGER, R .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 1989, 117 :33-43
[7]  
Colas D, 2004, THESIS U J MONNET SA
[8]  
Collins GS, 1996, NUOVO CIMENTO D, V18, P329, DOI 10.1007/BF02458913
[9]   Nickel and iron aluminides: An overview on properties, processing, and applications [J].
Deevi, SC ;
Sikka, VK .
INTERMETALLICS, 1996, 4 (05) :357-375
[10]   X-ray diffraction and Mossbauer spectrometry studies of the mechanically alloyed Fe-6P-1.7C powders [J].
Dekhil, L. ;
Alleg, S. ;
Sunol, J. J. ;
Greneche, J. M. .
ADVANCED POWDER TECHNOLOGY, 2009, 20 (06) :593-597