Effect of concentration of Al2(SO4)3•18H2O on the synthesis of nanosized alumina

被引:0
|
作者
Shaheen, F
Shah, WA
Mirza, ML
Iqbal, MP
机构
[1] Pakistan Council Sci & Ind Res, Glass & Ceram Res Ctr, Lahore, Pakistan
[2] Islamia Univ Bahawalpur, Dept Chem, Bahawalpur, Pakistan
来源
关键词
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Nanosized alumina has been prepared by the gelation of the solution containing aluminum sulphate and urea followed by low temperature calcination. The effect of different concentrations on pH and its ultimate effect on gelation were studied. Gel formation occurred in the solutions containing 1:20 salt/urea ratio. Aluminum hydroxide and nanoparticles of alumina were characterized by SEM, DTA and TG. The process describes the formation of aluminum hydroxide Al(OH)(3) and its thermal decomposition to Aluminum hydroxyoxide AlOOH and finally to aluminum oxide Al2O3. Nanoparticles of alumina produced were spherical with average particle size of 200 nm.
引用
收藏
页码:602 / 605
页数:4
相关论文
共 50 条
  • [21] Glass formation in the Al2(SO4)3-HIO3-H2O system
    Kirilenko, I.A.
    Kudinov, I.B.
    Azarova, L.A.
    2003, MAIK Nauka (48):
  • [22] Glass formation in the Al2(SO4)3-AlCl3-H2O system
    I. A. Kirilenko
    Russian Journal of Inorganic Chemistry, 2010, 55 : 1133 - 1135
  • [23] Glass formation in the Al2(SO4)3-AlCl3-H2O system
    Kirilenko, I. A.
    RUSSIAN JOURNAL OF INORGANIC CHEMISTRY, 2010, 55 (07) : 1133 - 1135
  • [24] Glass formation in the Al2(SO4)3-HIO3-H2O system
    Kirilenko, IA
    Kudinov, IB
    Azarova, LA
    RUSSIAN JOURNAL OF INORGANIC CHEMISTRY, 2003, 48 (09) : 1439 - 1441
  • [25] CHEMISM OF ALUMINUM PRECIPITATION IN THE AL2(SO4)3-NA2SO3-H2O SYSTEM
    MARGULIS, EV
    VOROPANOVA, LA
    BASHKOV, BI
    ZHURNAL NEORGANICHESKOI KHIMII, 1989, 34 (01): : 214 - 217
  • [26] FORMATION OF ALUMINA WHISKERS USING AL2(SO4)3 AND ALUMINUM ISOPROPOXIDE
    PATEL, M
    PADHI, BK
    JOURNAL OF MATERIALS SCIENCE LETTERS, 1991, 10 (21) : 1243 - 1245
  • [27] 85 DEGREES C ISOTHERM OF AL2(SO4)3 - H2SO4 - H2O SYSTEM
    BRETSZNAJDER, S
    ROJKOWSK.Z
    BULLETIN DE L ACADEMIE POLONAISE DES SCIENCES-SERIE DES SCIENCES CHIMIQUES, 1966, 14 (08): : 541 - +
  • [28] Thermodynamic Properties of Solutions in the H2O–Na2SO4–Al2(SO4)3 System
    A. V. Nesterov
    A. M. Demchenko
    A. A. Potashnikov
    A. L. Voskov
    N. A. Kovalenko
    I. A. Uspenskaya
    Russian Journal of Inorganic Chemistry, 2023, 68 : 195 - 201
  • [29] Mangazeite, Al2(SO4)(OH)4 · 3H2O, a new mineral species
    G. N. Gamyanin
    Yu. Ya. Zhdanov
    N. V. Zayakina
    V. V. Gamyanina
    V. S. Suknev
    Geology of Ore Deposits, 2007, 49 : 514 - 517
  • [30] Humidity dependent conductance of Al2(SO4)3&middot16H2O
    Chakraborty, Supratio
    Smart Materials and Structures, 1995, 4 (04): : 368 - 369