Synthesis and Characterization of N-[1,10-Phenanthroline]-N′-[(Benzo-15-Crown-5)yl] Thiourea and Its Complex with Copper(I)

被引：1

作者：

Elmali, Fikriye Tuncel ^{[1
]}

Avciata, Ulvi ^{[1
]}

Demirhan, Nebahat ^{[1
]}

Gul, Ahmet ^{[2
]}

机构：

[1] Yildiz Tech Univ, Fac Arts & Sci, Dept Chem, TR-34210 Esenler, Turkey

[2] Tech Univ Istanbul, Dept Chem, Istanbul, Turkey

来源：

INNOVATIONS IN CHEMICAL BIOLOGY | 2009年

关键词：

Copper; ligand; phenanthroline; thiourea; SODIUM; 1,10-PHENANTHROLINE;

D O I：

10.1007/978-1-4020-6955-0_43

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

A new thiourea ligand, N-[1,10-phenanthroline]-N'-[benzo-15-crown-5)yl]thiourea has been synthesized from the reaction of 5-amino-1,10-phenanthroline with 15-isothiocyanatobenzo[15-crown-5] and its Cu(I) complex has been prepared. The structures of the ligand and its complex have been characterized by elemental analysis, UV-vis, F-FIR, H-1 NMR (DMSO-d(6)), C-13 NMR (DMSO-d(6)) and MS spectra (LC-MS).

引用

页码：367 / +

页数：3

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