Analytical methods and problems related to the determination of organotin compounds in marine sediments

被引：13
作者：
Staniszewska, Marta [1 ]
Radke, Barbara [1 ]
Namiesnik, Jacek [2 ]
Bolalek, Jerzy [1 ]
机构：
[1] Univ Gdansk, Inst Oceanog, Dept Marine Chem & Environm Protect, Gdynia, Poland
[2] Gdansk Univ Technol, Fac Chem, Dept Analyt Chem, PL-80952 Gdansk, Poland
来源：
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY | 2008年 / 88卷 / 11期
关键词：
organotin compounds; marine sediments; speciation analysis;
D O I：
10.1080/03067310802082310
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
The determination of organotin compounds in bottom sediments is a complex process that requires a number of analytical steps, i.e. sample collection, transport and storage; extraction of analytes from sediment; derivatization; extract purification; enrichment; and the final chromatographic measurement. The whole process is time and labour consuming, and subject to securing sample representativeness. In this review the most frequently encountered problems and the examples of possible analytical solutions are presented, which encompass the specific steps of speciation analysis of these toxic compounds.
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收藏
页码：747 / 774
页数：28
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