Novel 9-nickelafluorenyl sandwich complexes of nickel(II) and cobalt(II)

被引：13

作者：

Buchalski, Piotr ^{[1
]}

Grabowska, Ilona ^{[1
]}

Karaskiewicz, Anna ^{[1
]}

Suwinska, Kinga ^{[2
]}

Jerzykiewicz, Lucjan ^{[3
]}

机构：

[1] Warsaw Univ Technol, Fac Chem, PL-00662 Warsaw, Poland

[2] Polish Acad Sci, Inst Phys Chem, PL-01224 Warsaw, Poland

[3] Univ Wroclaw, Fac Chem, PL-50353 Wroclaw, Poland

来源：

ORGANOMETALLICS | 2008年 / 27卷 / 13期

关键词：

D O I：

10.1021/om8002834

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

(9-Nickelafluorenyl)lithium was found to react with Ni(II) and Co(II) salts to form novel complexes in which the Ni or Co central metal atom is bonded to two nickelafluorenyl ligands. The crystal and molecular structures of the products were determined by single-crystal X-ray analysis.

引用

收藏

页码：3316 / 3319

页数：4

相关论文

共 29 条

[1] SECONDARY BONDING IN ORGANOBISMUTH COMPOUNDS - COMPARISON OF THE STRUCTURES OF 2,2',5,5'-TETRAMETHYL-1,1'-DIBISMAFERROCENE AND 2,2',5,5'-TETRAMETHYLBIBISMOLE [J].

ASHE, AJ ;

KAMPF, JW ;

PURANIK, DB ;

ALTAWEEL, SM .

ORGANOMETALLICS, 1992, 11 (08) :2743-2745

[2] CONFORMATIONS OF HETEROFERROCENES - SYNTHESIS AND CRYSTAL AND DYNAMIC SOLUTION BEHAVIOR OF 2,2',5,5'-TETRAKIS(TRIMETHYLSILYL)-3,3',4,4'-TETRAMETHYL-1,1'-DISTIBAFERROCENE [J].

ASHE, AJ ;

KAMPF, JW ;

ALTAWEEL, SM .

ORGANOMETALLICS, 1992, 11 (04) :1491-1496

[3] SECONDARY BONDING IN ORGANOPNICOGEN COMPOUNDS - COMPARISON OF THE STRUCTURES OF OCTAMETHYL-1,1'-DISTIBAFERROCENE AND OCTAMETHYL-1,1'-DIARSAFERROCENE [J].

ASHE, AJ ;

KAMPF, JW ;

PILOTEK, S ;

ROUSSEAU, R .

ORGANOMETALLICS, 1994, 13 (10) :4067-4071

[4] MOLECULAR AND CRYSTAL-STRUCTURE OF 2,2',5,5'-TETRAMETHYL-1,1'-DISTIBAFERROCENE - A SHORT SB=SB INTER-RING CONTACT [J].

ASHE, AJ ;

DIEPHOUSE, TR ;

KAMPF, JW ;

ALTAWEEL, SM .

ORGANOMETALLICS, 1991, 10 (06) :2068-2071

[5]

BALLWEG D, 2002, SILICON CHEM, V0001

[6] TANTALUM-BOROLLIDE ALKYL COMPLEXES [J].

BAZAN, GC ;

ROGRIGUEZ, G .

POLYHEDRON, 1995, 14 (01) :93-102

[7] Interactions in crystals.: 139.: Biphenylene ring expansion by a (H3C)2Si link from silicone grease as proven by the crystal structures of [(sodium+[2.2.1]cryptand)(9,9-dimethylsilafluorene•-)] as well as [sodium+(triglyme)2(biphenylene•-)] and by total-reflection X-ray fluroescence spectrometry (TXRF) [J].

Bock, H ;

Sievert, M ;

Bogdan, CL ;

Kolbesen, BO ;

Wittershagen, A .

ORGANOMETALLICS, 1999, 18 (12) :2387-2389

[8]

Braun S, 2000, 150 and More Basic NMR Experiments: A Practical Course Second Expanded Edition

[9] Synthesis and structures of 9-nickelafluorenyllithium complexes [J].

Buchalski, Piotr ;

Grabowska, Ilona ;

Kaminska, Elzbieta ;

Suwinska, Kinga .

ORGANOMETALLICS, 2008, 27 (10) :2346-2349

[10] TEMPERATURE DEPENDENT MAGNETIC MEASUREMENTS AND STRUCTURAL EQUILIBRIA IN SOLUTION [J].

CRAWFORD, TH ;

SWANSON, J .

JOURNAL OF CHEMICAL EDUCATION, 1971, 48 (06) :382-&