Microstructure, electrical and mechanical properties of MgO nanoparticles-reinforced porous PZT 95/5 ferroelectric ceramics

被引:22
作者
Wang, Junxia [1 ,2 ]
Nie, Hengchang [1 ]
Lan, Chunfeng [1 ]
Wang, Genshui [1 ]
Dong, Xianlin [1 ]
Chen, Xuefeng [1 ]
Cao, Fei [1 ]
He, Hongliang [3 ]
机构
[1] Chinese Acad Sci, Shanghai Inst Ceram, Key Lab Inorgan Funct Mat & Devices, Shanghai 200050, Peoples R China
[2] Southwest Univ Sci & Technol, State Key Lab Cultivat Base Nonmet Composite & Fu, Mianyang 621010, Peoples R China
[3] CAEP, Inst Fluid Phys, Lab Shock Wave & Detonat Phys Res, Mianyang 621900, Peoples R China
关键词
PZT/MgO; Microstructure; Electrical properties; Mechanical properties; PHASE-TRANSFORMATION; NANOCOMPOSITES; POROSITY; FABRICATION;
D O I
10.1016/j.ceramint.2012.10.238
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Porous Pb (Zr0.95Ti0.05) O-3/xMgO (PZT/MgO, x=0, 0.1, 0.2, 0.5 and 1.0 wt%) ferroelectric ceramics were prepared with MgO nanoparticles as reinforcing phase. The effects of MgO nanoparticles on the phase, microstructure, electrical and mechanical properties of as-prepared ceramics were investigated. The results show that the grain size is reduced obviously when increasing the amount of MgO. Compared with pure porous PZT, T-C of MgO-added PZT ceramics shifts to higher temperature. Moreover, dielectric, ferroelectric and piezoelectric properties show no much degradation. Further, PZT/MgO ceramics possess enhanced mechanical properties compared to pure porous PZT ceramics, the largest increment of the fracture toughness and hardness being 31.3% and 19.8%, respectively. The optimal electrical and mechanical properties are obtained with the addition of less than 0.5 wt% MgO nanoparticles. (C) 2012 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:3915 / 3919
页数:5
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