Synthesis and characterization of large WO3 sheets synthesized by resistive heating method

被引:1
作者
Filippo, Emanuela [1 ]
Tepore, Marco [1 ]
Baldassarre, Francesca [2 ]
Quarta, Gianluca [1 ]
Calcagnile, Lucio [1 ]
Guascito, Maria Rachele [3 ]
Tepore, Antonio [2 ]
机构
[1] Univ Salento, Dept Engn Innovat, I-73100 Lecce, Italy
[2] Univ Salento, Dept Cultural Heritage, I-73100 Lecce, Italy
[3] Univ Salento, DiSTeBA, I-73100 Lecce, Italy
关键词
Oxides; Heat treatment; Electron microscopy; Electron diffraction; TUNGSTEN-OXIDE NANOWIRES; THIN-FILMS; SENSING CHARACTERISTICS; GAS; NANOSTRUCTURES; PERFORMANCE; NANORODS; SENSOR; PHOTOANODE; SUBSTRATE;
D O I
10.1016/j.matchemphys.2015.09.007
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A simple, low-cost method is presented to grow tungsten oxide large sheets simply by resistively heating a pure tungsten filament under air/water vapor flow. The obtained structures were studied using scanning and transmission electron microscopy, selected area diffraction, X Ray diffraction, Raman and X-ray photoelectron spectroscopy, photoluminescence and zeta potential measurements. SEM observations revealed that sheets formed by broadening of the wires/belts over longer growth period. Photoluminescence measurements showed that tungsten oxide sheets had an intense visible emission band. (C) 2015 Published by Elsevier B.V.
引用
收藏
页码:134 / 141
页数:8
相关论文
共 50 条
  • [21] Synthesis, Characterization, and Gas Sensing Applications of WO3 Nanobricks
    Xiao, Jingkun
    Song, Chengwen
    Dong, Wei
    Li, Chen
    Yin, Yanyan
    Zhang, Xiaoni
    Song, Mingyan
    JOURNAL OF MATERIALS ENGINEERING AND PERFORMANCE, 2015, 24 (08) : 3026 - 3031
  • [22] Synthesis of WO3 nanoparticles for biosensing applications
    Santos, Lidia
    Silveira, Celia M.
    Elangovan, Elamurugu
    Neto, Joana P.
    Nunes, Daniela
    Pereira, Luis
    Martins, Rodrigo
    Viegas, Jaime
    Moura, Jose J. G.
    Todorovic, Smilja
    Gabriela Almeida, M.
    Fortunato, Elvira
    SENSORS AND ACTUATORS B-CHEMICAL, 2016, 223 : 186 - 194
  • [23] Fabrication and characterization of WO3 films by an electrophoretic deposition method
    Park, Yoon-Tae
    Lee, Ki-Tae
    JOURNAL OF CERAMIC PROCESSING RESEARCH, 2012, 13 (05): : 607 - 611
  • [24] Synthesis and characterization of WO3 nanowires and metal nanoparticle-WO3 nanowire composites
    Szabo, Maria
    Pusztai, Peter
    Leino, Anne-Riikka
    Kordas, Krisztian
    Konya, Zoltan
    Kukovecz, Akos
    JOURNAL OF MOLECULAR STRUCTURE, 2013, 1044 : 99 - 103
  • [25] Monodisperse WO3 hierarchical spheres synthesized via a microwave assisted hydrothermal method: time dependent morphologies and gas sensing characterization
    Wang, Zhenyu
    Zhou, Xin
    Li, Zhubo
    Zhuo, Yichen
    Gao, Yuan
    Yang, Qiuyue
    Li, Xiaowei
    Lu, Geyu
    RSC ADVANCES, 2014, 4 (44) : 23281 - 23286
  • [26] Sub-ppm level NO2 sensing properties of polyethyleneimine-mediated WO3 nanoparticles synthesized by a one-pot hydrothermal method
    Li, Tingting
    Shen, Yanbai
    Zhao, Sikai
    Zhong, Xiangxi
    Zhang, Wei
    Han, Cong
    Wei, Dezhou
    Meng, Dan
    Ao, Yuxin
    JOURNAL OF ALLOYS AND COMPOUNDS, 2019, 783 : 103 - 112
  • [27] Synthesis of spherical WO3•H2O network for ethanol sensing application
    Liu, Shilin
    Zeng, Wen
    Li, Yanqiong
    MATERIALS LETTERS, 2019, 253 : 42 - 45
  • [28] Synthesis, formation mechanism and sensing properties of WO3 hydrate nanowire netted-spheres
    Yan, Aihua
    Xie, Changsheng
    Zeng, Dawen
    Cai, Shuizhou
    Hu, Mulin
    MATERIALS RESEARCH BULLETIN, 2010, 45 (10) : 1541 - 1547
  • [29] Effect of synthesis route on the structural and morphological properties of WO3 nanostructures
    Jamali, Mohaddeseh
    Tehrani, Fatemeh Shariatmadar
    MATERIALS SCIENCE IN SEMICONDUCTOR PROCESSING, 2020, 107
  • [30] Synthesis and Characterization of WO3 Thin Film by Spray Pyrolysis for Gas Sensing Application
    Aher, Yogesh B.
    Jain, Gotan H.
    Shinde, Sarika D.
    Mandawade, Abhinay S.
    Sonawane, Laxmi D.
    Patil, Dnyaneshwari Y.
    Ahemad, Huda I.
    Femi, Matthew D.
    More, Manoj A.
    Kajale, Dnyaneshwar D.
    Patil, Ganesh E.
    PHYSICS OF THE SOLID STATE, 2024, 66 (11) : 497 - 504