Synthesis and characterization of large WO3 sheets synthesized by resistive heating method

被引：1
|
作者：
Filippo, Emanuela [1 ]
Tepore, Marco [1 ]
Baldassarre, Francesca [2 ]
Quarta, Gianluca [1 ]
Calcagnile, Lucio [1 ]
Guascito, Maria Rachele [3 ]
Tepore, Antonio [2 ]
机构：
[1] Univ Salento, Dept Engn Innovat, I-73100 Lecce, Italy
[2] Univ Salento, Dept Cultural Heritage, I-73100 Lecce, Italy
[3] Univ Salento, DiSTeBA, I-73100 Lecce, Italy
来源：
MATERIALS CHEMISTRY AND PHYSICS | 2015年 / 165卷
关键词：
Oxides; Heat treatment; Electron microscopy; Electron diffraction; TUNGSTEN-OXIDE NANOWIRES; THIN-FILMS; SENSING CHARACTERISTICS; GAS; NANOSTRUCTURES; PERFORMANCE; NANORODS; SENSOR; PHOTOANODE; SUBSTRATE;
D O I：
10.1016/j.matchemphys.2015.09.007
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
A simple, low-cost method is presented to grow tungsten oxide large sheets simply by resistively heating a pure tungsten filament under air/water vapor flow. The obtained structures were studied using scanning and transmission electron microscopy, selected area diffraction, X Ray diffraction, Raman and X-ray photoelectron spectroscopy, photoluminescence and zeta potential measurements. SEM observations revealed that sheets formed by broadening of the wires/belts over longer growth period. Photoluminescence measurements showed that tungsten oxide sheets had an intense visible emission band. (C) 2015 Published by Elsevier B.V.
引用
收藏
页码：134 / 141
页数：8
相关论文
共 50 条
  • [1] Synthesis and characterization of WO3 nanostructures prepared by an aged-hydrothermal method
    Huirache-Acuna, R.
    Paraguay-Delgado, F.
    Albiter, M. A.
    Lara-Romero, J.
    Martinez-Sanchez, R.
    MATERIALS CHARACTERIZATION, 2009, 60 (09) : 932 - 937
  • [2] WO3 work function enhancement induced by filamentous films deposited by resistive heating evaporation technique
    Sanchez, Fabien
    Dmitriev, A.
    Antunes, R.
    Steiner, R.
    Meyer, E.
    JOURNAL OF ALLOYS AND COMPOUNDS, 2023, 968
  • [3] Synthesis and characterization of WO3 spherical nanoparticles and nanorods
    Adhikari, Sangeeta
    Sarkar, Debasish
    Maiti, Himadri Sekhar
    MATERIALS RESEARCH BULLETIN, 2014, 49 : 325 - 330
  • [4] Characterization and Modeling of WO3 Nanowires Synthesized via the Solvothermal Method: A Proposed 8-Pointed Star Prism Structure
    Gao, Chenjing
    Guo, Xingwu
    Wu, Xuan
    Peng, Li-Ming
    Chen, Juan
    CRYSTAL GROWTH & DESIGN, 2023, 23 (06) : 4410 - 4416
  • [5] Xanthate sensing properties of Pt-functionalized WO3 microspheres synthesized by one-pot hydrothermal method
    Li, Tingting
    Shen, Yanbai
    Zhao, Sikai
    Chen, Xiangxiang
    Li, Guodong
    Lu, Rui
    Zhu, Lijia
    Li, Hansen
    Wei, Dezhou
    Shen, Yansong
    CERAMICS INTERNATIONAL, 2018, 44 (05) : 4814 - 4823
  • [6] Room Temperature Polymorphism in WO3 Produced by Resistive Heating of W Wires
    Rodriguez, Beatriz
    Dolado, Jaime
    Lopez-Sanchez, Jesus
    Hidalgo, Pedro
    Mendez, Bianchi
    NANOMATERIALS, 2023, 13 (05)
  • [7] Hydrothermal synthesis and chromic properties of hexagonal WO3 nanowires
    Yuan Hua-Jun
    Chen Ya-Qi
    Yu Fang
    Peng Yue-Hua
    He Xiong-Wu
    Zhao Ding
    Tang Dong-Sheng
    CHINESE PHYSICS B, 2011, 20 (03)
  • [8] WO3 Nanoparticles in the 5-30 nm Range by Solvothermal Synthesis under Microwave or Resistive Heating
    Le Houx, N.
    Pourroy, G.
    Camerel, F.
    Comet, M.
    Spitzer, D.
    JOURNAL OF PHYSICAL CHEMISTRY C, 2010, 114 (01) : 155 - 161
  • [9] Combustion synthesized hierarchically porous WO3 for selective acetone sensing
    Dong, Chengjun
    Liu, Xu
    Guan, Hongtao
    Chen, Gang
    Xiao, Xuechun
    Djerdj, Igor
    Wang, Yude
    MATERIALS CHEMISTRY AND PHYSICS, 2016, 184 : 155 - 161
  • [10] Synthesis, Characterization, Photocatalysis, and Antibacterial Study of WO3, MXene and WO3/MXene Nanocomposite
    Warsi, Al-Zoha
    Aziz, Fatima
    Zulfiqar, Sonia
    Haider, Sajjad
    Shakir, Imran
    Agboola, Philips O.
    NANOMATERIALS, 2022, 12 (04)
12345