Preparation of magnesium ferrite nanoparticles by ultrasonic wave-assisted aqueous solution ball milling

被引：66

作者：

Chen, Ding ^{[1
]}

Li, Dian-yi ^{[1
]}

Zhang, Ying-zhe ^{[1
]}

Kang, Zhi-tao ^{[2
,3
]}

机构：

[1] Hunan Univ, Coll Mat Sci & Engn, Changsha 410082, Hunan, Peoples R China

[2] Georgia Inst Technol, Georgia Tech Res Inst, Atlanta, GA 30332 USA

[3] Georgia Inst Technol, Sch Mat Sci & Engn, Atlanta, GA 30332 USA

来源：

ULTRASONICS SONOCHEMISTRY | 2013年 / 20卷 / 06期

关键词：

Ultrasonic wave; Aqueous solution ball milling; Magnesium ferrite; Nanoparticle; MGFE2O4;

D O I：

10.1016/j.ultsonch.2013.04.001

中图分类号：

O42 [声学];

学科分类号：

070206 ; 082403 ;

摘要：

Magnesium ferrite, MgFe2O4 nanoparticles with high saturation magnetization were successfully synthesized using ultrasonic wave-assisted ball milling. In this study, the raw materials were 4MgCO(3)center dot Mg(OH)(2-)center dot 5H(2)O and Fe2O3 powders and the grinding media was stainless steel ball. The average particle diameter of the product MgFe2O4 powders was 20 nm and the saturation magnetization of them reached 54.8 emu/g. The different results of aqueous solution ball milling with and without ultrasonic wave revealed that it was the coupling effect of ultrasonic wave and mechanical force that played an important role during the synthesis of MgFe2O4. In addition, the effect of the frequency of the ultrasonic wave on the ball milling process was investigated. (C) 2013 Elsevier B.V. All rights reserved.

引用

页码：1337 / 1340

页数：4

共 26 条

[1] Bangale S. V., 2011, ARCH APPL SCI RES, V3
[2] Preparation of nanoscale MgFe2O4 via non-conventional mechanochemical route
Bergmann, I.
Sepelak, V.
Becker, K. D.
[J]. SOLID STATE IONICS, 2006, 177 (19-25) : 1865 - 1868
[3] Mechanochemistry: The mechanical activation of covalent bonds
Beyer, MK
Clausen-Schaumann, H
[J]. CHEMICAL REVIEWS, 2005, 105 (08) : 2921 - 2948
[4] Brebers V., 1995, HDB MAGNETIC MAT, V8
[5] Effect of Power and Frequency on Bubble-Size Distributions in Acoustic Cavitation
Brotchie, Adam
Grieser, Franz
Ashokkumar, Muthupandian
[J]. PHYSICAL REVIEW LETTERS, 2009, 102 (08)
[6] Candeia R. A., 2006, MAT RES BULLET, V41
[7] Preparation of high saturation magnetic MgFe2O4 nanoparticles by microwave-assisted ball milling
Chen, Ding
Zhang, Yingzhe
Tu, Chuanjun
[J]. MATERIALS LETTERS, 2012, 82 : 10 - 12
[8] One-step synthesis of manganese ferrite nanoparticles by ultrasonic wave-assisted ball milling technology
Chen, Ding
Liu, Hong Yan
Li, Lin
[J]. MATERIALS CHEMISTRY AND PHYSICS, 2012, 134 (2-3) : 921 - 924
[9] Chen N. S., 2000, SENS ACTUATORS B, V66
[10] Chen Q., 1996, J MAGN MAGN MATER, V194, P1

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