Preparation and characterization of mullite whisker reinforced ceramics made from coal fly ash

被引:44
作者
Li, Chaoxin [1 ]
Zhou, Yi [1 ]
Tian, Yuming [1 ,2 ]
Zhao, Yuanyuan [1 ]
Wang, Kaiyue [1 ]
Li, Guomin [1 ]
Chai, Yuesheng [1 ]
机构
[1] Taiyuan Univ Sci & Technol, Sch Mat Sci & Engn, Taiyuan, Shanxi, Peoples R China
[2] Shanxi Engn Vocat Coll, Taiyuan, Shanxi, Peoples R China
关键词
Coal fly ash; Mullite whisker; Pickling; Phase structure; Microstructure; HIGH-STRENGTH; SUPPORTS;
D O I
10.1016/j.ceramint.2018.12.021
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Ceramics with mullite whiskers were prepared from coal fly ash and Al2O3 raw materials, with AIF(3) used as an additive. The phase structures and microstructures of the ceramics were identified via X-ray diffraction and scanning electron microscopy, respectively. The results show that pickling of coal fly ash is an effective method for enhancing the flexural strength of ceramics. Sintering temperature and AlF3 addition were also key factors influencing the creation of ideal ceramics. The ceramic made from pickled coal fly ash, 6 wt% AlF3, and sintered at 1200 degrees C, exhibited the highest flexural strength of 59.1 MPa, and had a bulk density of 1.32 g/cm(3) and porosity of 26.8%. The results show that ceramic materials made under these conditions are ideal candidates for manufacturing ceramic proppants for the exploitation of unconventional oil and gas resources.
引用
收藏
页码:5613 / 5616
页数:4
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