An efficient protocol for synthesis of 4-methoxy cinnamate in ionic liquid

被引:0
作者
Wang, Yu Fang [1 ]
Yang, Qi Chao [1 ,2 ]
Zhang, Bao Ji [1 ]
Lin, Dong [1 ]
Zhang, Ming Jie [1 ]
机构
[1] Tianjin Univ, Dept Chem, Sch Sci, Tianjin 300072, Peoples R China
[2] Nanyang Normal Univ, Chem & Pharmaceut Engn Coll, Nanyang 473061, Peoples R China
关键词
2-Ethylhexyl-4-methoxy cinnamate; Heck reaction; ionic liquid; recycled; HECK REACTION; ARYL BROMIDES; CATALYST; PALLADIUM;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Synthesis of 2-ethylhexyl-4-methoxy cinnamate was carried out efficiently using palladium-catalyzed Heck reaction of 4-bromoanisole and 2-ethylhexylacrylate in tetrabutyl ammonium bromide-based ionic liquid. The ionic liquid was used as a cost,effective reaction medium and the catalyst in it is Stable and Can be recycled for at least four times Without significant lass in activity.
引用
收藏
页码:489 / 492
页数:4
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