X-ray diffractometer combining synchrotron radiation and pulsed magnetic fields up to 40 T

被引:44
作者
Narumi, Y [1 ]
Kindo, K
Katsumata, K
Kawauchi, M
Broennimann, C
Staub, U
Toyokawa, H
Tanaka, Y
Kikkawa, A
Yamamoto, T
Hagiwara, M
Ishikawa, T
Kitamura, H
机构
[1] Univ Tokyo, ISSP, Kashiwa, Chiba 277858, Japan
[2] RIKEN, SPring 8 Ctr, Harima Inst, Sayo, Hyogo 6795148, Japan
[3] Osaka Univ, KYOKUGEN, Toyonaka, Osaka 5608531, Japan
[4] Paul Scherrer Inst, Swiss Light Source, CH-5232 Villigen, Switzerland
[5] JASRI, SPring 8, Sayo, Hyogo 6795198, Japan
关键词
X-ray diffraction; pulsed high magnetic field; pixel detector; magnetostriction; antiferromagnet;
D O I
10.1107/S0909049506006972
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A synchrotron X-ray diffractometer incorporating a pulsed field magnet for high fields up to 40 T has been developed and a detailed description of this instrument is reported. The pulsed field magnet is composed of two coaxial coils with a gap of 3 mm at the mid-plane for passage of the X-rays. The pixel detector PILATUS 100K is used to store the diffracted X-rays. As a test of this instrument, X-ray diffraction by a powder sample of the antiferromagnet CoO is measured below the Neel temperature. A field-dependent lattice distortion of CoO due to magnetostriction is observed up to 38 T.
引用
收藏
页码:271 / 274
页数:4
相关论文
共 12 条
[1]  
Berthier C., 2002, HIGH MAGNETIC FIELDS
[2]   The brightest x-ray source:: A very long undulator at SPring-8 [J].
Hara, T ;
Yabashi, M ;
Tanaka, T ;
Bizen, T ;
Goto, S ;
Maréchal, XM ;
Seike, T ;
Tamasaku, K ;
Ishikawa, T ;
Kitamura, H .
REVIEW OF SCIENTIFIC INSTRUMENTS, 2002, 73 (03) :1125-1128
[3]  
Herlach F., 2003, HIGH MAGNETIC FIELDS, VI.
[4]   Distortion calibration of the PILATUS 1M detector [J].
Hülsen, G ;
Brönnimann, C ;
Eikenberry, EF .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2005, 548 (03) :540-554
[5]  
KANAMORI J, 1963, MAGNETISM, V1, P189
[6]   Synchrotron X-ray diffraction studies of magnetic materials under extreme conditions [J].
Katsumata, K .
PHYSICA SCRIPTA, 2005, 71 (02) :CC7-CC13
[7]   100T magnet developed in Osaka [J].
Kindo, K .
PHYSICA B, 2001, 294 :585-590
[8]   Application of a portable pulsed magnet to synchrotron radiation experiments [J].
Matsuda, YH ;
Ueda, Y ;
Nojiri, H ;
Takahashi, T ;
Inami, T ;
Ohwada, K ;
Murakami, Y ;
Arima, T .
PHYSICA B-CONDENSED MATTER, 2004, 346 :519-523
[10]   STRUCTURE OF MONOXIDES OF SOME TRANSITION ELEMENTS AT LOW TEMPERATURES [J].
TOMBS, NC ;
ROOKSBY, HP .
NATURE, 1950, 165 (4194) :442-443