Synthesis and crystal structure of tert-butyl 4-[(E)-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-1-butenyl] benzoate

被引：0
|
作者：
Zhang, XG [1 ]
Zhang, HJ [1 ]
Wang, Z [1 ]
Li, CX [1 ]
机构：
[1] Nankai Univ, Inst Polymer Chem, Tianjin 300071, Peoples R China
来源：
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2006年 / 25卷 / 03期
关键词：
tert-butyl 4-[(E)-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-1-butenyl]benzoate; synthesis; crystal structure;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The title compound tert-butyl 4-[(E)-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)1-butenyl] benzoate has been synthesized and characterized by X-ray crystallography. It crystallizes in monoclinic, space group C-2/c with a = 14.875(3), b = 8.979603), c = 34.736(6) Alpha, beta = 95.981(4)degrees, V = 4614.4(14) angstrom(3), Z = 8, D-c = 1.213 g/cm(3), F(000) = 1792, mu(MoKa) = 0.084 mm(-1), R = 0.0602 and wR = 0.1445 for 4613 unique reflections with 2272 observed ones (I > 2 sigma(I)). The results of crystal structure determination show that the title compound has a layer structure, and the two benzene rings in molecule are parallel to each other.
引用
收藏
页码：300 / 304
页数：5
相关论文
共 50 条
  • [31] Synthesis and Properties of 4-(2,5-Dihydro-2,5-dioxo-1H-pyrrol-1-yl)benzenesulfonamide
    O. A. Kolyamshin
    Yu. N. Mitrasov
    A. A. Avruyskaya
    V. A. Danilov
    Yu. Yu. Pyl’chikova
    Russian Journal of General Chemistry, 2023, 93 : S472 - S477
  • [32] Synthesis and Properties of 4-(2,5-Dihydro-2,5-dioxo-1H-pyrrol-1-yl)benzenesulfonamide
    Kolyamshin, O. A.
    Mitrasov, Yu. N.
    Avruyskaya, A. A.
    Danilov, V. A.
    Pyl'chikova, Yu. Yu.
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2023, 93 (SUPPL 2) : S472 - S477
  • [33] (E)-tert-Butyl 2-(5-{[4-(dimethylamino)phenyl] diazenyl}-2,6-dioxo-1H-pyrimid-in-3-yl) acetate dichloromethane monosolvate
    Hudson, Robert H. E.
    Moustafa, Mohamed E.
    Boyle, Paul D.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O556 - +
  • [34] 4-[(1,3-Dioxoisoindolin-2-yl)methyl]benzenesulfonamide
    Mague, Joel T.
    Abdel-Aziz, Alaa A. -M.
    El-Azab, Adel S.
    EI-Sherbeny, Magda A.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O291 - +
  • [35] Crystal structure of 2-oxopyrrolidin-3-yl 4-(2-phenyldiazen-1-yl)benzoate
    Elkin, Igor
    Maris, Thierry
    Melkoumov, Alexandre
    Hildgen, Patrice
    Banquy, Xavier
    Leclair, Gregoire
    Barrett, Christopher
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2018, 74 : 458 - +
  • [36] Crystal structure of 2-(4-(2-butyl-1,3-dioxo-2,3-dihydro-1H-benzo[de]isoquinolin-6-yl)piperazin-1-yl)-2-oxoethyldiethylcarbamodithioate, C27H34N4O3S2
    Liu, Ya-Tong
    Kang, Lei
    Li, Na-Na
    Xing, Zhi-Yong
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2017, 232 (02): : 295 - 296
  • [37] Crystal structure of ethyl 4-[(1H-pyrazol-1-yl)methyl]benzoate
    Wang, Ju-Xian
    Feng, Chao
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O1287 - +
  • [38] Condensed phase conformational isomerisation of 5-[3-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-propoxy]-3-methyl-1-phenyl-1H-pyrazole-4-carboxylic acid methyl ester
    Tewari, Ashish K.
    Srivastava, Priyanka
    Singh, Ved P.
    Puerta, Carmen
    Valerga, Pedro
    ARKIVOC, 2010, : 127 - 136
  • [39] Synthesis of 4-(1H-1,2,3-Triazol-4-YL)-1,3-Thiazole-2-Amine Derivatives
    Bunev, A. S.
    Trushkova, Yu. O.
    Ostapenko, G. I.
    Statsyuk, V. E.
    Peregudov, A. S.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2014, 50 (07) : 1027 - 1031
  • [40] Methyl 4-[(2-butyl-4-chloro-5-formyl-1H-imidazol-1-yl)methyl]benzoate
    Yang, FK
    Xiao, HL
    Jian, FF
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2004, 60 : O2266 - O2267
12345