Synthesis and crystal structure of tert-butyl 4-[(E)-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-1-butenyl] benzoate

被引：0
|
作者：
Zhang, XG [1 ]
Zhang, HJ [1 ]
Wang, Z [1 ]
Li, CX [1 ]
机构：
[1] Nankai Univ, Inst Polymer Chem, Tianjin 300071, Peoples R China
来源：
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2006年 / 25卷 / 03期
关键词：
tert-butyl 4-[(E)-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-1-butenyl]benzoate; synthesis; crystal structure;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The title compound tert-butyl 4-[(E)-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)1-butenyl] benzoate has been synthesized and characterized by X-ray crystallography. It crystallizes in monoclinic, space group C-2/c with a = 14.875(3), b = 8.979603), c = 34.736(6) Alpha, beta = 95.981(4)degrees, V = 4614.4(14) angstrom(3), Z = 8, D-c = 1.213 g/cm(3), F(000) = 1792, mu(MoKa) = 0.084 mm(-1), R = 0.0602 and wR = 0.1445 for 4613 unique reflections with 2272 observed ones (I > 2 sigma(I)). The results of crystal structure determination show that the title compound has a layer structure, and the two benzene rings in molecule are parallel to each other.
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页码：300 / 304
页数：5
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