Synthesis and crystal structure of tert-butyl 4-[(E)-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-1-butenyl] benzoate

被引：0
|
作者：
Zhang, XG [1 ]
Zhang, HJ [1 ]
Wang, Z [1 ]
Li, CX [1 ]
机构：
[1] Nankai Univ, Inst Polymer Chem, Tianjin 300071, Peoples R China
来源：
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2006年 / 25卷 / 03期
关键词：
tert-butyl 4-[(E)-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-1-butenyl]benzoate; synthesis; crystal structure;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The title compound tert-butyl 4-[(E)-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)1-butenyl] benzoate has been synthesized and characterized by X-ray crystallography. It crystallizes in monoclinic, space group C-2/c with a = 14.875(3), b = 8.979603), c = 34.736(6) Alpha, beta = 95.981(4)degrees, V = 4614.4(14) angstrom(3), Z = 8, D-c = 1.213 g/cm(3), F(000) = 1792, mu(MoKa) = 0.084 mm(-1), R = 0.0602 and wR = 0.1445 for 4613 unique reflections with 2272 observed ones (I > 2 sigma(I)). The results of crystal structure determination show that the title compound has a layer structure, and the two benzene rings in molecule are parallel to each other.
引用
收藏
页码：300 / 304
页数：5
相关论文
共 50 条
  • [1] Synthesis and Crystal Structure of Tert-butyl 4-[(E)-4-(1,3-Dioxo-1,3-dihydro-2H-isoindol-2-yl)-1-butenyl] Benzoate
    张新歌
    张慧杰
    王瑱
    李朝兴
    Chinese Journal of Structural Chemistry, 2006, (03) : 300 - 304
  • [2] Crystal Structures of (2-oxo-2H-Quinaxalin-1-yl)-acetic Acid and its Cobalt and Nickel Complexes and Their Comparison with (1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-acetic Acid
    Anirban Karmakar
    Jubaraj B. Baruah
    Journal of Chemical Crystallography, 2008, 38 : 485 - 489
  • [3] Crystal structures of (2-oxo-2H-quinaxalin-1-yl)-acetic acid and its cobalt and nickel complexes and their comparison with (1,3-dioxo-1,3-dihydro-isoindol-2-yl)-acetic acid
    Karmakar, Anirban
    Baruah, Jubaraj B.
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2008, 38 (06) : 485 - 489
  • [4] Crystal structure of tert-butyl 4[4-(4-fluorophenyl)-2-methylbut-3-yn-2-yl]piperazine-1-carboxylate
    Gumireddy, Ashwini
    DeBoyace, Kevin
    Rupprecht, Alexander
    Gupta, Mohit
    Patel, Saloni
    Flaherty, Patrick T.
    Wildfong, Peter L. D.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2021, 77 : 360 - +
  • [5] Synthesis, crystal structure, vibrational spectral and density functional studies of 4-(1,3-dioxoisoindolin-2-yl)antipyrine
    Yu, Zongxue
    Sun, Gang
    Liu, Zengwei
    Yu, Cheng
    Huang, Changliang
    Sun, Yuxi
    JOURNAL OF MOLECULAR STRUCTURE, 2012, 1030 : 113 - 124
  • [6] Synthesis of (Tert-butyl)-3-(methyl)-4-(4-(methylthio)benzyl) piperazine-1,3-dicarboxylate
    Feng, Baicheng
    Xu, Wen
    Chu, Xiaodong
    Li, Chunyang
    Jin, Yan
    INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2018, 28 (04) : 503 - 505
  • [7] Synthesis, crystal structure and DFT study of tert-butyl 4-(5-bromopyridin-2-yloxy)piperidine-1-carboxylate
    Hou, Yuanyuan
    Wu, Qingmei
    Chen, Yumei
    Ye, Wenjun
    Wang, Sisi
    Zhao, Chunshen
    Zhou, Zhixu
    MOLECULAR CRYSTALS AND LIQUID CRYSTALS, 2023, 767 (01) : 147 - 158
  • [8] Crystal structure of diethyl {2,2,2-trichloro-1-[2-(1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl)-4-methyl-pentanamido]ethyl}phosphonate
    Brovarets, V. S.
    Golovchenko, O. V.
    Rusanov, E. B.
    Rusanova, J. A.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2018, 74 : 915 - +
  • [9] Crystal structure of 2-oxopyrrolidin-3-yl 4-(2-phenyldiazen-1-yl)benzoate
    Elkin, Igor
    Maris, Thierry
    Melkoumov, Alexandre
    Hildgen, Patrice
    Banquy, Xavier
    Leclair, Gregoire
    Barrett, Christopher
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2018, 74 : 458 - +
  • [10] Crystal structure of ethyl 4-[(1H-pyrazol-1-yl)methyl]benzoate
    Wang, Ju-Xian
    Feng, Chao
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O1287 - +
12345