Transmission electron microscopy characterization of microstructure and TiN precipitation in low-energy nitrogen ion implanted V-Ti alloys

被引:0
作者
Ortíz, MI [1 ]
García, JA [1 ]
Varela, M [1 ]
Rivière, JP [1 ]
Rodríguez, R [1 ]
Ballesteros, C [1 ]
机构
[1] Univ Politecn Madrid, Dept Tecnol Elect, ETSIT, E-28040 Madrid, Spain
来源
THIN FILMS STRESSES AND MECHANICAL PROPERTIES XI | 2005年 / 875卷
关键词
D O I
暂无
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
A detailed structural characterization of low-energy, nitrogen implanted V5at.%Ti alloys is presented. Samples were nitrogen-implanted at 1.2 kV and 1 mA/cm(2), up to a dose of 4x10(-19) ions/cm(2), at temperatures between 400-575 degrees C. Alloys were analysed by transmission electron microscopy. Depending on the implantation temperature, the ion beam treatment dramatically changes the microstructure of the material. Partial amorphization, nitride precipitation and dislocations are imaged. A clear correlation between the microstructure of the implanted layer and the reported improvement in the tribological properties has been demonstrated. For implantation at 575 degrees C a nanocomposite layer forms at the sample surface, where the reinforcement particles are TiN precipitates.
引用
收藏
页码:403 / 408
页数:6
相关论文
共 50 条
[41]   CHARACTERIZATION OF OXYGEN-ION-IMPLANTED SILICON USING SPECTROSCOPIC ELLIPSOMETRY AND TRANSMISSION ELECTRON-MICROSCOPY [J].
LYNCH, S ;
CREEN, GM ;
GREEF, R ;
MARGAIL, J ;
LAMURE, JM ;
STOEMENOS, J .
MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY, 1992, 12 (1-2) :173-176
[42]   TRANSMISSION ELECTRON-MICROSCOPY OBSERVATIONS OF LOW-TEMPERATURE ION-IMPLANTED (100) SILICON [J].
SERVIDORI, M ;
VECCHI, I .
SOLID-STATE ELECTRONICS, 1981, 24 (04) :329-331
[43]   Depth profile characterization of low-energy B+- and Ge+-ion-implanted Si [J].
Karmakov, I ;
Chakarov, I ;
Konova, A .
APPLIED SURFACE SCIENCE, 2003, 211 (1-4) :270-279
[44]   Corrosion resistance of plasma-based low-energy nitrogen ion implanted austenitic stainless steel [J].
Lei, MK ;
Zhu, XM .
CONTRIBUTIONS OF SURFACE ENGINEERING TO MODERN MANUFACTURING AND REMANUFACTURING, 2002, :384-387
[45]   Characterization of precipitates in Ti-stabilized steels with low-energy electron-induced X-ray spectrometry and scanning electron microscopy [J].
Geyer, J ;
Flock, J ;
Broekaert, JAC .
MIKROCHIMICA ACTA, 1999, 131 (3-4) :191-197
[46]   Characterization of Precipitates in Ti-Stabilized Steels with Low-Energy Electron-Induced X-Ray Spectrometry and Scanning Electron Microscopy [J].
Jutta Geyer ;
Jörg Flock ;
Jośe A. C. Broekaert .
Microchimica Acta, 1999, 131 :191-197
[47]   Characterization of metal alloy systems by scanning tunneling microscopy and low-energy ion backscattering [J].
Niehus, H .
PHYSICA STATUS SOLIDI B-BASIC RESEARCH, 1995, 192 (02) :357-374
[48]   Characterization of hexagonal boron nitride layers on nickel surfaces by low-energy electron microscopy [J].
Mende, P. C. ;
Gao, Q. ;
Ismach, A. ;
Chou, H. ;
Widom, M. ;
Ruoff, R. ;
Colombo, L. ;
Feenstra, R. M. .
SURFACE SCIENCE, 2017, 659 :31-42
[49]   Silicone-based modified layer obtained by low-energy nitrogen ion beam as diaphragm for environmental transmission electron microscope [J].
Tai, Yuki ;
Matsutani, Takaomi ;
Kawasaki, Tadahiro .
SURFACE & COATINGS TECHNOLOGY, 2020, 385
[50]   Transmission electron microscopy studies of microstructure of Ti-Nb and Ti-Ta alloys after ball milling and hot consolidation [J].
Maziarz, W. ;
Lejkowska, M. ;
Michalski, A. ;
Dutkiewicz, J. .
JOURNAL OF MICROSCOPY, 2006, 224 :42-45