Platelet growth of mercuric iodide

被引：3

作者：

McGregor, Douglas S. ^{[1
]}

Ariesanti, Elsa ^{[2
]}

机构：

[1] Kansas State Univ, Dept Mech & Nucl Engn, SMART Lab, Manhattan, KS 66506 USA

[2] Radiat Monitoring Devices, Watertown, MA 02472 USA

来源：

JOURNAL OF CRYSTAL GROWTH | 2013年 / 379卷

关键词：

Growth from vapor; Semiconducting mercury compounds; FRISCH COLLAR DETECTORS; HGI2; FABRICATION; POLYMORPHS; PROGRAM;

D O I：

10.1016/j.jcrysgro.2013.03.001

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The Faile growth method, when used with purified mercuric iodide (HgI2), along with low molecular weight polyethylene, has yielded tetragonal prismatic HgI2 crystals. Thermal desorption-gas chromatography/mass spectroscopy (TD-GC/MS) studies reveal the existence of alkanes and ketones in the growth ampoules along with low molecular weight polyethylene, presumably decomposition byproducts from, or impurities in, the polyethylene. The influence of these desorbed byproducts on the HgI2 crystal morphology is compared to the basic Bravais-Friedel-Donnay-Harker (BFDH) crystal model. From these comparisons, it is apparent that ketones assert the most influence on the HgI2 crystal morphology by slowing the growth of the {110} faces, thereby, causing the tetragonal prismatic crystal shapes to grow. (c) 2013 Elsevier B.V. All rights reserved.

引用

页码：7 / 15

页数：9

共 22 条

[1] MERCURIC IODIDE CRYSTAL GROWTH AND FRISCH COLLAR DETECTOR FABRICATION [J].

Ariesanti, E. ;

Kargar, A. ;

McGregor, D. S. .

NUCLEAR TECHNOLOGY, 2011, 175 (01) :124-130

[2] Fabrication and spectroscopy results of mercuric iodide Frisch collar detectors [J].

Ariesanti, E. ;

Kargar, A. ;

McGregor, D. S. .

NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2010, 624 (03) :656-661

[3]

Ariesanti E., 2011, THESIS KANSAS STATE

[4]

Ariesanti E., 2008, P SPIE, V7079

[5] THE ROLE OF POLYETHYLENE IN PLATELET GROWTH OF MERCURIC IODIDE [J].

BURGER, A ;

ROTH, M ;

SCHIEBER, M .

JOURNAL OF CRYSTAL GROWTH, 1982, 56 (02) :526-531

[6] YIELD AND QUALITY OF HGI2 VAPOR GROWN PLATELETS [J].

BURGER, A ;

LEVI, A ;

NISSENBAUM, J ;

ROTH, M ;

SCHIEBER, M .

JOURNAL OF CRYSTAL GROWTH, 1985, 72 (03) :643-648

[7]

Faile S. P., 1980, US patent, Patent No. [4,282,057, 4282057]

[8] MERCURIC IODIDE (HGI2) PLATELETS FOR X-RAY SPECTROSCOPY PRODUCED BY POLYMER CONTROLLED GROWTH [J].

FAILE, SP ;

DABROWSKI, AJ ;

HUTH, GC ;

IWANCZYK, JS .

JOURNAL OF CRYSTAL GROWTH, 1980, 50 (03) :752-756

[9]

Hartman P., 1973, Crystal Growth: an Introduction

[10] Phase diagrams and structures of HgX2 (X = I, Br, Cl, F) [J].

Hostettler, M ;

Schwarzenbach, D .

COMPTES RENDUS CHIMIE, 2005, 8 (02) :147-156

← 1 2 3 →