Reactions of N-sulfinyltrifluoromethanesulfonamide with carboxylic acids

被引：5
|
作者：
Shainyan, B. A. [1 ]
Tolstikova, L. L. [1 ]
Bel'skikh, A. V. [1 ]
机构：
[1] Russian Acad Sci, Favorskii Irkutsk Inst Chem, Siberian Div, Irkutsk 664033, Russia
来源：
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2008年 / 44卷 / 08期
基金：
俄罗斯基础研究基金会;
关键词：
Carboxy Group; Thionyl Chloride; Acetohydrazide; Methanesulfonamide; Trifluoromethanesulfonamide;
D O I：
10.1134/S1070428008080022
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Phenylacetic, diphenylacetic, salicylic, and cinnamic acids reacted with N-sulfinyltrifluoromethanesulfonamide (CF3SO2NSO) to give the corresponding N-acyltrifluoromethanesulfonamides CF3SO2NHCOR (R = PhCH2, Ph2CH, o-HOC6H4, PhCH=CH). The reaction of N-sulfinyl-trifluoromethanesulfonamide with 3-hydrazinobenzoic acid Occurred at the hydrazino group of the latter with conservation of the carboxy group and without elimination of SO2, and the product was 3-(2-sulfinylhydrazino)benzoic acid OSNNHC6H4CO2H.
引用
收藏
页码：1121 / 1125
页数：5
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