Effect of ultrasonic radiation's times to the control size of silver nanoparticles in κ-carrageenan

被引：12
|
作者：
Elsupikhe, Randa Fawzi [1 ]
Shameli, Kamyar [2 ]
Ahmad, Mansor B. [1 ]
机构：
[1] Univ Putra Malaysia, Dept Chem, Fac Sci, Serdang 43400, Selangor, Malaysia
[2] Univ Teknol Malaysia, Malaysia Japan Int Inst Technol MJIIT, Kuala Lumpur 54100, Malaysia
来源：
RESEARCH ON CHEMICAL INTERMEDIATES | 2015年 / 41卷 / 11期
关键词：
Green method; Ultrasonic irradiation; Silver nanoparticles; kappa-Carrageenan; Silver nitrate; GLASSY-CARBON; REDUCTION; RELEASE;
D O I：
10.1007/s11164-015-1931-7
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The sonochemical method as a green method for the preparation and size control of silver nanoparticles (Ag-NPs) formed in kappa-carrageenan has been developed. kappa-carrageenan was chosen because it is an eco-friendly stabilizer and ultrasonic irradiation reducing agent. Formations of Ag/kappa-carrageenan were determined by electronic spectroscopy where the surface plasmon absorption maxima were observed at 437-412 nm. The FT-IR spectrum indicated the presence of kappa-carrageenan in capping with Ag-NPs. The XRD analysis proved that the Ag-NPs were of a face-centered cubic structure. TEM images displayed well-dispersed Ag-NPs with an average particle size of less than 10 nm. SEM images indicated the spherical shape of the Ag-NPs.
引用
收藏
页码：8829 / 8838
页数：10
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