Synthesis and characterization of chiral catenanes based on rigid calix[4]arene

被引：8
|
作者：
Okada, Y [1 ]
Miao, ZH
Akiba, M
Nishimura, J
机构：
[1] Gunma Univ, Dept Chem, Kiryu, Gumma 3768515, Japan
[2] Gunma Univ, Dept Nanomat Syst, Kiryu, Gumma 3768515, Japan
来源：
TETRAHEDRON LETTERS | 2006年 / 47卷 / 16期
关键词：
calixarene; catenane; enantiomer; circular dichroism;
D O I：
10.1016/j.tetlet.2006.02.083
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A new class of chiral calix[4]arene-based [2]catenanes was synthesized in excellent yields of 51-80%. They exhibit unique dynamic properties according to variable temperature NMR experiments. The enantiomeric pure (+)-catenane was prepared in 66% yield starting from (-)-calix[4]arene. (c) 2006 Elsevier Ltd. All rights reserved.
引用
收藏
页码：2699 / 2702
页数：4
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