Backside-illuminated scientific CMOS detector for soft X-ray resonant scattering and ptychography

被引:30
作者
Desjardins, Kewin [1 ]
Medjoubi, Kadda [1 ]
Sacchi, Maurizio [1 ]
Popescu, Horia [1 ]
Gaudemer, Roland [1 ]
Belkhou, Rachid [1 ]
Stanescu, Stefan [1 ]
Swaraj, Sufal [1 ]
Besson, Adrien [1 ]
Vijayakumar, Jaianth [1 ]
Pautard, Stephanie [1 ]
Noureddine, Arafat [1 ]
Mercere, Pascal [1 ]
Da Silva, Paulo [1 ]
Orsini, Fabienne [1 ]
Menneglier, Claude [1 ]
Jaouen, Nicolas [1 ]
机构
[1] Synchrotron SOLEIL, F-91192 Gif Sur Yvette, France
关键词
X-ray detectors; sCMOS camera; 2D soft X-ray detector; soft X-ray scattering; ptychography; back-illuminated CMOS; quantum efficiency; radiation hardness; coherent diffraction; PERFORMANCE;
D O I
10.1107/S160057752001262X
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
The impressive progress in the performance of synchrotron radiation sources is nowadays driven by the so-called 'ultimate storage ring' projects which promise an unprecedented improvement in brightness. Progress on the detector side has not always been at the same pace, especially as far as soft X-ray 2D detectors are concerned. While the most commonly used detectors are still based on microchannel plates or CCD technology, recent developments of CMOS (complementary metal oxide semiconductor)-type detectors will play an ever more important role as 2D detectors in the soft X-ray range. This paper describes the capabilities and performance of a camera equipped with a newly commercialized backside-illuminated scientific CMOS (sCMOS-BSI) sensor, integrated in a vacuum environment, for soft X-ray experiments at synchrotron sources. The 4 Mpixel sensor reaches a frame rate of up to 48 frames s(-1) while matching the requirements for X-ray experiments in terms of high-intensity linearity (>98%), good spatial homogeneity (<1%), high charge capacity (up to 80 ke(-)), and low readout noise (down to 2 e(-) r.m.s.) and dark current (3 e(-) per second per pixel). Performance evaluations in the soft X-ray range have been carried out at the METROLOGIE beamline of the SOLEIL synchrotron. The quantum efficiency, spatial resolution (24 line-pairs mm(-1)), energy resolution (<100 eV) and radiation damage versus the X-ray dose (<600 Gy) have been measured in the energy range from 40 to 2000 eV. In order to illustrate the capabilities of this new sCMOS-BSI sensor, several experiments have been performed at the SEXTANTS and HERMES soft X-ray beamlines of the SOLEIL synchrotron: acquisition of a coherent diffraction pattern from a pinhole at 186 eV, a scattering experiment from a nanostructured Co/Cu multilayer at 767 eV and ptychographic imaging in transmission at 706 eV.
引用
收藏
页码:1577 / 1589
页数:13
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