[1] Leibniz Inst Solid State & Mat Res Dresden, D-01171 Dresden, Germany
[2] Diamond Light Source Ltd, Didcot OX11 0DE, Oxon, England
[3] Natl Acad Sci Ukraine, Inst Met Phys, UA-03142 Kiev, Ukraine
[4] Moscow MV Lomonosov State Univ, Dept Chem, Moscow 119991, Russia
[5] Tech Univ Dresden, Inst Festkorperphys, D-01171 Dresden, Germany