Determination of iron and lead by flame atomic absorption spectrometry after preconcentration with sepiolite

被引:33
作者
Turker, AR [1 ]
Bag, H [1 ]
Erdogan, B [1 ]
机构
[1] KIRIKKALE UNIV,FEN EDEBIYAT FAK,TR-71200 KIRIKKALE,TURKEY
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1997年 / 357卷 / 03期
关键词
D O I
10.1007/s002160050166
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
By using a new adsorbent (sepiolite) an adsorption-elution and atomic absorption spectrometric method has been developed for the preconcentration and determination of Fe and Pb. Recoveries of the analytes were 82 +/- 3% for Fe and 91 +/- 2% for Pb at 95% confidence level. For Cu it was only 5 +/- 1%. The recovery of iron could be increased to about 97 +/- 1% by complexing with EDTA, the recovery of copper only to 57 +/- 2%. The optimised method was applied to the determination of lead in metal materials (e.g. brass).
引用
收藏
页码:351 / 353
页数:3
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