Coupling of Electron Channeling with EBSD: Toward the Quantitative Characterization of Deformation Structures in the SEM

被引:101
作者
Gutierrez-Urrutia, I. [1 ]
Zaefferer, S. [1 ]
Raabe, D. [1 ]
机构
[1] Max Planck Inst Eisenforsch GmbH, D-40237 Dusseldorf, Germany
关键词
COPPER SINGLE-CRYSTALS; BACKSCATTERED ELECTRONS; DISLOCATION DENSITIES; BULK MATERIALS; CONTRAST; MICROSCOPY; PATTERNS; DIFFRACTION; PLASTICITY; RESOLUTION;
D O I
10.1007/s11837-013-0678-0
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The coupling of electron channeling contrast imaging (ECCI) with electron backscatter diffraction (EBSD) provides an efficient and fast approach to perform ECCI of crystal defects, such as dislocations, cells, and stacking faults, under controlled diffraction conditions with enhanced contrast. From a technical point of view, the ECCI technique complements two of the main electron microscopy techniques, namely, EBSD and conventional diffraction-based transmission electron microscopy. In this review, we provide several application examples of the EBSD-based ECCI approach on microstructure characterization, namely, characterization of single dislocations, measurement of dislocation densities, and characterization of dislocation substructures in deformed bulk materials. We make use of a two-beam Bloch wave approach to interpret the channeling contrast associated with crystal defects. The approach captures the main features observed in the experimental contrast associated with stacking faults and dislocations.
引用
收藏
页码:1229 / 1236
页数:8
相关论文
共 56 条
  • [1] [Anonymous], 2008, Springer Ser. Opt. Sci.
  • [2] Ayache J., 2009, SAMPLE PREPARATION H
  • [3] KIKUCHI-LIKE REFLECTION PATTERNS OBTAINED WITH SCANNING ELECTRON MICROSCOPE
    COATES, DG
    [J]. PHILOSOPHICAL MAGAZINE, 1967, 16 (144): : 1179 - &
  • [4] Demonstration of the g•b x u=0 edge dislocation invisibility criterion for electron channelling contrast imaging
    Crimp, MA
    Simkin, BA
    Ng, BC
    [J]. PHILOSOPHICAL MAGAZINE LETTERS, 2001, 81 (12) : 833 - 837
  • [5] Scanning electron microscopy imaging of dislocations in bulk materials, using electron channeling contrast
    Crimp, Martin A.
    [J]. MICROSCOPY RESEARCH AND TECHNIQUE, 2006, 69 (05) : 374 - 381
  • [6] IMAGING OF DISLOCATIONS USING BACKSCATTERED ELECTRONS IN A SCANNING ELECTRON-MICROSCOPE
    CZERNUSZKA, JT
    LONG, NJ
    BOYES, ED
    HIRSCH, PB
    [J]. PHILOSOPHICAL MAGAZINE LETTERS, 1990, 62 (04) : 227 - 232
  • [7] Investigation of the indentation size effect through the measurement of the geometrically necessary dislocations beneath small indents of different depths using EBSD tomography
    Demir, Eralp
    Raabe, Dierk
    Zaafarani, Nader
    Zaefferer, Stefan
    [J]. ACTA MATERIALIA, 2009, 57 (02) : 559 - 569
  • [8] THEORY OF ELECTRON BACKSCATTERING FROM CRYSTALS
    DUDAREV, SL
    REZ, P
    WHELAN, MJ
    [J]. PHYSICAL REVIEW B, 1995, 51 (06): : 3397 - 3412
  • [9] Adiabatic temperature increase associated with deformation twinning and dislocation plasticity
    Eisenlohr, A.
    Gutierrez-Urrutia, I.
    Raabe, D.
    [J]. ACTA MATERIALIA, 2012, 60 (09) : 3994 - 4004
  • [10] Analysis of local orientation gradients in deformed single crystals
    Field, DP
    Trivedi, PB
    Wright, SI
    Kumar, M
    [J]. ULTRAMICROSCOPY, 2005, 103 (01) : 33 - 39