Preparation and characterization of surface reactable modified silver nanoparticles

被引:0
作者
He Ben-Fang [1 ]
Zhang Sheng-Mao [1 ]
Zhang Lin-Na [1 ]
Zhou Hui [1 ]
Zhang Ping-Yu [1 ]
Wu Zhi-Shen [1 ]
机构
[1] Henan Univ, Lab Special Funct Mat, Kaifeng 475001, Henan, Peoples R China
关键词
surface reactable modified; silver nanoparticles; O; O '-di(11-bromic undecane)dithiophosphonic acid;
D O I
暂无
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Surface reactable modified silver nanoparticles were prepared by NaBH4 reduced silver ion in the aquenous solvent, in the presence of the double group modifying agent, O,O'-di(11-bromic undecane)dithiophosphonic acid. The morphology and structure of the product were characterized using Transmission Electron Microscope(TEM), UV-Visible Absorption(UV-Vis) spectra, Fourier Transform Infrared(FTIR) spectra. The result indicate that the products are spherical shape and no aggregation, C-Br functional groups are on the outermost portion of the silver nanoparticles. The nanoparticles were well dispersed in organic solution, such as chloroform, petroleum ether, toluene etc. The analysis of the sample which reacted with trimethylamine by X-ray photoelectron spectra(XPS) shows the silver nanoparticles can undergo many reactions.
引用
收藏
页码:921 / 924
页数:4
相关论文
共 15 条
[1]   Selectively assembled Co nanoparticle stripes prepared by covalent linkage and microcontact printing [J].
Bae, SS ;
Lim, DK ;
Park, JI ;
Lee, WR ;
Cheon, J ;
Kim, S .
JOURNAL OF PHYSICAL CHEMISTRY B, 2004, 108 (08) :2575-2579
[2]   Effects of size dispersion disorder on the charge transport in self-assembled 2-D Ag nanoparticle arrays [J].
Beverly, KC ;
Sampaio, JF ;
Heath, JR .
JOURNAL OF PHYSICAL CHEMISTRY B, 2002, 106 (09) :2131-2135
[3]  
Chen HJ, 2005, CHINESE J INORG CHEM, V21, P241
[4]   Study of a nanocomposite based on a conducting polymer:: Polyaniline [J].
Kohut- Svelko, N ;
Reynaud, S ;
Dedryvère, R ;
Martinez, H ;
Gonbeau, D ;
François, J .
LANGMUIR, 2005, 21 (04) :1575-1583
[5]   Microwave-polyol process for Pt and Ag nanoparticles [J].
Komarneni, S ;
Li, DS ;
Newalkar, B ;
Katsuki, H ;
Bhalla, AS .
LANGMUIR, 2002, 18 (15) :5959-5962
[6]   Facile synthesis of silver nanoparticles useful for fabrication of high-conductivity elements for printed electronics [J].
Li, YN ;
Wu, YL ;
Ong, BS .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2005, 127 (10) :3266-3267
[7]  
LINDBERG BJ, 1975, CHEM SCRIPTA, V7, P155
[8]   High-density silver nanoparticle film with temperature-controllable interparticle spacing for a tunable surface enhanced Raman scattering substrate [J].
Lu, Y ;
Liu, GL ;
Lee, LP .
NANO LETTERS, 2005, 5 (01) :5-9
[9]   Formation of PVP-protected metal nanoparticles in DMF [J].
Pastoriza-Santos, I ;
Liz-Marzán, LM .
LANGMUIR, 2002, 18 (07) :2888-2894
[10]   Adsorption of potassium O,O′-Di(para-fluorophenyl) dithiophosphate on gold, silver, and copper [J].
Persson, NO ;
Uvdal, K ;
Almquist, O ;
Engquist, I ;
Kariis, H ;
Liedberg, B .
LANGMUIR, 1999, 15 (23) :8161-8169